孟加拉拉杰沙希六个市场冬季蔬菜的农药残留分析

S. Begum, S. Sultana, Ahmed, M. Azad
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引用次数: 1

摘要

蔬菜中的农药残留已成为食品安全问题的主要关注点。2019年1月,在孟加拉国拉杰沙希地区的六个市场收集了豆类、茄子、番茄、花椰菜和卷心菜等五种冬季蔬菜。采用气相色谱-火焰热离子检测器(GC-FTD)方法测定了冬季蔬菜样品中常用农药(甲胺磷、乐果、二嗪农、灭虫硫磷、马拉硫磷、毒死蜱和喹乐磷)的残留量。采用醋酸缓冲快速、简便、廉价、有效、可靠、安全的QuEChERS方法(AOAC官方方法2007.01)制备样品。在30个样本中,农药残留仅在一个茄子和两个西红柿样本中发现。结果表明,在拉杰沙希市沙赫布集市和哈尔哈里集市采集的番茄样品中,乐果残留量分别为0.047 mg/kg和0.139 mg/kg。采自拉杰沙希沙尔巴甘集市的茄子样品,乐果残留量为0.052 mg/kg。3份样品的农药残留量均高于最大残留量(0.01 mg/kg)。
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Pesticide Residue Analysis from Winter Vegetables Collected from Six Markets of Rajshahi Bangladesh
Pesticide residues in vegetables have become a major concern associated with food safety issues. Five types of winter vegetables like bean, brinjal, tomato, cauliflower and cabbage were collected from six markets of Rajshahi District during January, 2019 in Bangladesh. Residues of commonly used pesticides (Acephate, Dimethoate, Diazinon, Fenotrothion, Malathion, Chlorpyrifos and Quinalphos) in winter vegetable samples were determined using Gas Chromatography-Flame Thermionic Detector (GC-FTD) procedures. A quick, easy, cheap, effective, rugged and safe (QuEChERS) method with acetate buffering (AOAC Official Method 2007.01) was used for sample preparation. Out of 30 samples, pesticide residues were found only in one brinjal and two tomato samples. The result showed that tomato samples collected from Shaheb bazar and Kharkhari bazar of Rajshahi City contained 0.047 mg/kg and 0.139 mg/kg dimethoate residue, respectively. Brinjal sample collected from Shalbagan bazar, Rajshahi, contained 0.052 mg/kg dimethoate residues. The detected pesticide residue dimethoate of these three samples was higher than maximum residue level (0.01 mg/kg).
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