沙柳枝热解酸的制备、化学成分及抑菌活性

Jingjing Li, Xi Ma, Haiyan Duan
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引用次数: 1

摘要

为了提高沙柳废弃物的附加值,在90 ~ 380℃和380 ~ 550℃两个温度范围内对沙柳枝中的热解酸进行了提取。对其化学成分和抑菌活性进行了详细的研究。GC-MS结果表明,从这两种PAs中鉴定出34个化合物。90 ~ 380℃时,PA的主要成分为有机酸类和酮类,380 ~ 550℃时,PA的主要成分为有机酸类和酚类。在380 ~ 550℃时,PA的总酸和酚类物质含量高达67.96%,具有较强的抗菌活性。两种PAs均对5种病原菌和2种致病菌具有良好的抑菌活性,其中对大丽花黄萎病菌的抑菌活性最强。与90 ~ 380℃的抑菌活性相比,380 ~ 550℃的抑菌活性更强,但对尖孢镰刀菌的抑菌活性较弱。
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PREPARATION, CHEMICAL CONSTITUENTS AND ANTIMICROBIAL ACTIVITY OF PYROLIGNEOUS ACIDS FROM SALIX PSAMMOPHILA BRANCHES
In order to improve the additional values of Salix psammophilabio-waste, pyroligneous acids (PAs) from Salix psammophila branches were extracted by thepyrolysis process at two temperature ranges: 90-380°C and 380-550°C. The chemical constituents and antimicrobial activities of PAs were investigated in detail. The GC-MS results showed that 34 compounds were identified from the two kinds of PAs. The main components were organic acids and ketones for PA at 90-380°C, while they were organic acids and phenols for PA at 380-550°C. The total content ofacids and phenols was as high as 67.96% for PA at 380-550°C, which contributed to the strong antimicrobial activity. Two PAs both showed good antimicrobial activities for five pathogenic fungi and two pathogenic bacteria, especially against Verticillium dahlia.Compared with the antimicrobial activity of PA at 90-380°C, PA at 380-550°C showed greater antifungal activity but against Fusarium oxysporum.
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