{"title":"绿色化学方法合成cuo纳米结构","authors":"Pourahmad Afshin","doi":"10.7508/IJND.2016.02.003","DOIUrl":null,"url":null,"abstract":"Molecular sieves MCM-41 were synthesized from rice husk ash (RHA) as alternative sources of silica. e material was synthesized by a room temperature method from a gel with the molar composition SiO 2 : 1.6 EA: 0.215HDTMABr: 325H 2 O with pH correction. The cetyltrimethylammonium bromide (CTMABr) was used as a structure template. Nanocomposite containing 5.0 and 10.0 wt.% of Cu was synthesized under solid state reaction. e calcinations of samples were done at two different temperatures, 400 and 600 ° C. The morphology and the physicochemical properties of the prepared samples were investigated by X-ray diffraction (XRD), UV-Vis diffuse reflectance spectroscopy (UV-Vis DRS), Fourier transform infrared spectroscopy (FTIR) and transmission electron microscopy (TEM). TEM images indicated that nanoparticles size of CuO is ~ 3 nm.","PeriodicalId":14081,"journal":{"name":"international journal of nano dimension","volume":null,"pages":null},"PeriodicalIF":1.2000,"publicationDate":"2016-05-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"3","resultStr":"{\"title\":\"GREEN CHEMISTRY APPROACH FOR THE SYNTHESIS OF CUO NANOSTRUCTURE\",\"authors\":\"Pourahmad Afshin\",\"doi\":\"10.7508/IJND.2016.02.003\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Molecular sieves MCM-41 were synthesized from rice husk ash (RHA) as alternative sources of silica. e material was synthesized by a room temperature method from a gel with the molar composition SiO 2 : 1.6 EA: 0.215HDTMABr: 325H 2 O with pH correction. The cetyltrimethylammonium bromide (CTMABr) was used as a structure template. Nanocomposite containing 5.0 and 10.0 wt.% of Cu was synthesized under solid state reaction. e calcinations of samples were done at two different temperatures, 400 and 600 ° C. The morphology and the physicochemical properties of the prepared samples were investigated by X-ray diffraction (XRD), UV-Vis diffuse reflectance spectroscopy (UV-Vis DRS), Fourier transform infrared spectroscopy (FTIR) and transmission electron microscopy (TEM). TEM images indicated that nanoparticles size of CuO is ~ 3 nm.\",\"PeriodicalId\":14081,\"journal\":{\"name\":\"international journal of nano dimension\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":1.2000,\"publicationDate\":\"2016-05-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"3\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"international journal of nano dimension\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.7508/IJND.2016.02.003\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"NANOSCIENCE & NANOTECHNOLOGY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"international journal of nano dimension","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.7508/IJND.2016.02.003","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"NANOSCIENCE & NANOTECHNOLOGY","Score":null,"Total":0}
GREEN CHEMISTRY APPROACH FOR THE SYNTHESIS OF CUO NANOSTRUCTURE
Molecular sieves MCM-41 were synthesized from rice husk ash (RHA) as alternative sources of silica. e material was synthesized by a room temperature method from a gel with the molar composition SiO 2 : 1.6 EA: 0.215HDTMABr: 325H 2 O with pH correction. The cetyltrimethylammonium bromide (CTMABr) was used as a structure template. Nanocomposite containing 5.0 and 10.0 wt.% of Cu was synthesized under solid state reaction. e calcinations of samples were done at two different temperatures, 400 and 600 ° C. The morphology and the physicochemical properties of the prepared samples were investigated by X-ray diffraction (XRD), UV-Vis diffuse reflectance spectroscopy (UV-Vis DRS), Fourier transform infrared spectroscopy (FTIR) and transmission electron microscopy (TEM). TEM images indicated that nanoparticles size of CuO is ~ 3 nm.