不同的应用方式是否提高了自蚀刻陶瓷底漆与二硅酸锂和长石陶瓷的结合性能?

A. Cardenas, Angela Sisley Quintero-Calderon, F. Siqueira, V. S. Campos, M. Wendlinger, Camilo Andres Pulido-Mora, María José Masson-Palacios, Martha Lucia Sarmiento-Delgado, A. Loguércio
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引用次数: 10

摘要

目的研究新型自蚀刻陶瓷底漆不同使用方式对两种玻璃陶瓷表面微剪切结合强度(μSBS)和陶瓷表面蚀刻图案的影响。材料与方法将22块二硅酸锂(LD)和长石玻璃陶瓷(VTR)的CAD/CAM块分别切割成4个矩形截面(陶瓷表面n = 88)。将LD和VTR样品分为1个对照组(氢氟酸+硅烷偶联剂[HF+SII])和10个实验组(使用Monobond Etch and Prime (MEP)),分别进行5、10、20、40和60 s的洗涤时间和20或40 s的反应时间组合)。每次处理后,将Tygon基质(n = 8)填充树脂水泥并对每个陶瓷样品进行光固化。37℃水中保存24 h,进行μSBS试验。对失败模式和μSBS进行统计学评价(α = 0.05)。此外,利用扫描电镜分析了陶瓷表面的蚀刻图案。结果在LD组中,MEP 60/40的平均μSBS高于HF+SI (p < 0.05)。5/40、10/40和20/40组的平均μSBS与HF+SI组相近(p > 0.05)。VTR组间差异无统计学意义(p = 0.32)。与MEP相比,HF能更好地促进两种陶瓷玻璃基体的溶解。然而,长时间的MEP擦洗或反应导致了两种评价陶瓷的玻璃基体的显著溶解。结论积极和长期应用MEP可替代HF+SI提高与LD的结合强度。
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Do Different Application Modes Improve the Bonding Performance of Self-etching Ceramic Primer to Lithium Disilicate and Feldspathic Ceramics?
PURPOSE To evaluate the effect of different application modes of a recently introduced self-etching ceramic primer on the microshear bond strength (μSBS) and ceramic surface-etching pattern of two glass-ceramic surfaces. MATERIALS AND METHODS Twenty-two CAD/CAM blocks of lithium disilicate (LD) and feldspathic glass ceramic (VTR) were each cut into 4 rectangular sections (n = 88 for ceramic surface). The LD and VTR specimens were divided into one control group (hydrofluoric acid + silane coupling agent [HF+SII]), and 10 experimental groups using Monobond Etch and Prime (MEP) applied for a combination of scrubbing times (5, 10, 20, 40, and 60 s) and reaction times (20 or 40 s). After each treatment, Tygon matrices (n = 8) were filled with a resin cement and light cured for each ceramic specimen. The specimens were stored in water at 37°C for 24 h and subjected to the μSBS test. The failure pattern and μSBS were statistically evaluated (α = 0.05). In addition, the ceramic surface etching pattern was analyzed using scanning electron microscopy. RESULTS For the LD groups, the application of MEP 60/40 resulted in a higher mean μSBS compared to HF+SI (p < 0.05). Groups 5/40, 10/40, and 20/40 resulted in mean μSBS similar to that obtained by HF+SI (p > 0.05). For VTR, no significant difference was observed among the groups (p = 0.32). Compared with MEP, HF better promoted the dissolution of glass matrix for both ceramics. However, prolonged MEP scrubbing or reaction caused significant dissolution of the glass matrix for both evaluated ceramics. CONCLUSION Active and prolonged application of MEP may be a viable alternative to HF+SI for increasing the bond strength to LD.
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