简单加热法制备稻壳纳米二氧化硅及其表征

IF 0.4 Q4 NANOSCIENCE & NANOTECHNOLOGY Nano Hybrids and Composites Pub Date : 2022-04-05 DOI:10.4028/p-9wx28g
S. Wibowo, Achmad Nandang Roziafanto, Ichsan Farizi, A. P. Tirta, Arifur Rahman, A. Subagio
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引用次数: 0

摘要

以稻壳灰为原料,采用简单的加热法制备了纳米二氧化硅。采用x射线衍射仪(XRD)、傅里叶红外变换仪(FTIR)、扫描电镜(SEM)和同步热分析(STA)等技术对所制得的纳米二氧化硅进行了表征。产品呈白色,表明不含碳或其他元素等杂质。XRD分析表明,所制得的纳米二氧化硅具有非晶二氧化硅材料的形态。红外光谱证实了纳米二氧化硅中的Si-O- si键和Si-O键。SEM图像显示纳米二氧化硅颗粒的团聚,平均直径约为12 nm。实验表明,在加热过程中,需要酸处理来去除纳米二氧化硅中的碳或金属元素。这些结果为利用稻壳以一种简单的方法转化为其他更有价值的产品提供了重要的支持。
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Nanosilica from Rice Husk Synthesized by a Simple Heating Method and its Characterization
Nanosilica from rice husk ash (RHA) has been synthesized by a simple heating method. The obtained nanosilica was characterized by several techniques such as x-ray diffractometer (XRD), Fourirer transform infrared (FTIR), scanning electron microscope (SEM), and simultaneous thermal analysis (STA). The products had white color indicating that there were no impurities such as carbon or other elements. The XRD showed that the obtained nanosilica exhibited the pattern of amorphous silica material. FTIR spectra confirmed Si-O-Si and Si-O bonds in the obtained nanosilica. SEM images displayed the agglomeration of nanosilica particles with the average diameter of about 12 nm. STA showed that acid treatment was needed to remove carbon or mettalic ellements from nanosilica during the heating process. These results were important in supporting the utilization of rice husk to convert into other more valuable products with a simple method.
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Nano Hybrids and Composites
Nano Hybrids and Composites NANOSCIENCE & NANOTECHNOLOGY-
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