András Kovács, Roland Schierholz, Karsten Tillmann
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引用次数: 111

摘要

FEI Titan G2 80-200 CREWLEY是第四代透射电子显微镜,专为研究在原子尺度上发生的各种固体现象而设计,包括结构和化学成分。为此,FEI Titan G2 80-200 CREWLEY配备了一个Schottky型高亮度电子枪(FEI X-FEG),一个Cs探针校正器(CEOS DCOR),一个柱内Super-X能量色散x射线光谱复制(EDX)单元(化学技术),一个柱后能量过滤系统(Gatan Enfinium ER 977),具有双电子能量损失光谱(EELS)选项,允许以每秒1000个光谱的速度同时读取EDX和EELS信号。为了记录数据,显微镜配备了角暗场(ADF)扫描TEM (STEM)探测器(Fischione Model 3000),轴上三重BF, DF1, DF2探测器,轴上BF/DF Gatan探测器以及400万像素CCD系统(Gatan UltraScan 1000 XP-P)。该仪器的典型使用示例和技术规格如下。
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FEI Titan G2 80-200 CREWLEY
The FEI Titan G2 80-200 CREWLEY is a fourth generation transmission electron microscope which has been specifically designed for the investigation of a wide range of solid state phenomena taking place on the atomic scale of both the structure and chemical composition. For these purposes, the FEI Titan G2 80-200 CREWLEY is equipped with a Schottky type high-brightness electron gun (FEI X-FEG), a Cs probe corrector (CEOS DCOR), an in-column Super-X energy dispersive X-ray spectros-copy (EDX) unit (ChemiSTEM technology), a post-column energy filter system (Gatan Enfinium ER 977) with dual electron energy-loss spectroscopy (EELS) option allowing a simultaneous read-out of EDX and EELS signals at a speed of 1000 spectra per second. For data recording the microscope is equipped with an angular dark-field (ADF) scanning TEM (STEM) detector (Fischione Model 3000), on-axis triple BF, DF1, DF2 detectors, on-axis BF/DF Gatan detectors as well as a 4 megapixel CCD system (Gatan UltraScan 1000 XP-P). Typical examples of use and technical specifications for the instrument are given below.
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