傅里叶变换红外(FTIR)分析刚果非食用牛蒡子油中脂肪酸甲酯的含量

A. Mulula, Thierno N. Manoka, E. B. Bayindu, A. Bouzina
{"title":"傅里叶变换红外(FTIR)分析刚果非食用牛蒡子油中脂肪酸甲酯的含量","authors":"A. Mulula, Thierno N. Manoka, E. B. Bayindu, A. Bouzina","doi":"10.9734/ajacr/2022/v11i430262","DOIUrl":null,"url":null,"abstract":"As the oils used for biodiesel production face food competition, many scientific research is now focusing on the upgrading of non-conventional oils, which are not edibles. This study consisted in revalorizing of Congolese nonedible Afzelia bella seeds oil as raw materials for the biodiesel production. Afzelia bella seeds oil was extracted with oil yield of 26.38±0.22% and subsequently transesterified by alkali-catalyst using methanol with KOH as catalyst. The maximum yield of the obtained Diacetylenic Light Fuel Oil was 96.53% and FTIR spectroscopy showed the presence of fatty acid methyl esters in the produced biodiesel. The FTIR spectrum of Diacetylenic Light Fuel Oil revealed the following characteristics functional groups: Carbonyl group stretching (C=O), Methyl asymmetric bending (CH3) and Methoxy group stretching (O-CH3) with the peaks at 1743.94, 1436.11 and 1197.38 cm-1, respectively. Physicochemical properties (Kinematic viscosity, density, flash point, Cetane number, cloud point, pour point, water contents, ash and sulfur contents) values of Biodiesel (B100), and biodiesel blend in Gasoil (B50 and B20), were within the range of values set by the international standards specifications of diesel and biodiesel (American Society of Testing Materials and European Standard). Thus, these three produced biodiesels (B100, B50 and B20) from the Congolese Afzelia bella seeds oil could be used as a substitute for diesel without damaging the engine.","PeriodicalId":8480,"journal":{"name":"Asian Journal of Applied Chemistry Research","volume":"16 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2022-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Fourier Transform Infrared (FTIR) Analysis of Fatty Acid Methyl Ester from Congolese Non-Edible Afzelia bella Seeds Oil\",\"authors\":\"A. Mulula, Thierno N. Manoka, E. B. Bayindu, A. Bouzina\",\"doi\":\"10.9734/ajacr/2022/v11i430262\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"As the oils used for biodiesel production face food competition, many scientific research is now focusing on the upgrading of non-conventional oils, which are not edibles. This study consisted in revalorizing of Congolese nonedible Afzelia bella seeds oil as raw materials for the biodiesel production. Afzelia bella seeds oil was extracted with oil yield of 26.38±0.22% and subsequently transesterified by alkali-catalyst using methanol with KOH as catalyst. The maximum yield of the obtained Diacetylenic Light Fuel Oil was 96.53% and FTIR spectroscopy showed the presence of fatty acid methyl esters in the produced biodiesel. The FTIR spectrum of Diacetylenic Light Fuel Oil revealed the following characteristics functional groups: Carbonyl group stretching (C=O), Methyl asymmetric bending (CH3) and Methoxy group stretching (O-CH3) with the peaks at 1743.94, 1436.11 and 1197.38 cm-1, respectively. Physicochemical properties (Kinematic viscosity, density, flash point, Cetane number, cloud point, pour point, water contents, ash and sulfur contents) values of Biodiesel (B100), and biodiesel blend in Gasoil (B50 and B20), were within the range of values set by the international standards specifications of diesel and biodiesel (American Society of Testing Materials and European Standard). Thus, these three produced biodiesels (B100, B50 and B20) from the Congolese Afzelia bella seeds oil could be used as a substitute for diesel without damaging the engine.\",\"PeriodicalId\":8480,\"journal\":{\"name\":\"Asian Journal of Applied Chemistry Research\",\"volume\":\"16 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2022-09-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Asian Journal of Applied Chemistry Research\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.9734/ajacr/2022/v11i430262\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Asian Journal of Applied Chemistry Research","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.9734/ajacr/2022/v11i430262","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0

摘要

由于用于生产生物柴油的油面临食品竞争,许多科学研究现在都把重点放在了非传统油的升级换代上。本研究包括重新评估刚果不可食用的阿兹利亚籽油作为生物柴油生产的原料。以产油率26.38±0.22%为原料,以KOH为催化剂,甲醇为原料,进行碱催化酯交换反应。所得二乙基轻燃料油的收率最高可达96.53%,FTIR光谱分析表明,所得生物柴油中存在脂肪酸甲酯。二乙基轻燃料油的FTIR光谱特征官能团为羰基拉伸(C=O)、甲基不对称弯曲(CH3)和甲氧基拉伸(O-CH3),其峰分别位于1743.94、1436.11和1197.38 cm-1。生物柴油的理化性质(运动粘度、密度、闪点、十六烷数、浊点、倾点、含水量、灰分和硫含量)值(B100)和生物柴油在汽油中的混合物(B50和B20)均在柴油和生物柴油国际标准规范(美国试验材料学会和欧洲标准)规定的范围内。因此,这三种生产的生物柴油(B100, B50和B20)从刚果阿兹利亚贝亚种子油可以用作柴油的替代品,而不会损坏发动机。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
Fourier Transform Infrared (FTIR) Analysis of Fatty Acid Methyl Ester from Congolese Non-Edible Afzelia bella Seeds Oil
As the oils used for biodiesel production face food competition, many scientific research is now focusing on the upgrading of non-conventional oils, which are not edibles. This study consisted in revalorizing of Congolese nonedible Afzelia bella seeds oil as raw materials for the biodiesel production. Afzelia bella seeds oil was extracted with oil yield of 26.38±0.22% and subsequently transesterified by alkali-catalyst using methanol with KOH as catalyst. The maximum yield of the obtained Diacetylenic Light Fuel Oil was 96.53% and FTIR spectroscopy showed the presence of fatty acid methyl esters in the produced biodiesel. The FTIR spectrum of Diacetylenic Light Fuel Oil revealed the following characteristics functional groups: Carbonyl group stretching (C=O), Methyl asymmetric bending (CH3) and Methoxy group stretching (O-CH3) with the peaks at 1743.94, 1436.11 and 1197.38 cm-1, respectively. Physicochemical properties (Kinematic viscosity, density, flash point, Cetane number, cloud point, pour point, water contents, ash and sulfur contents) values of Biodiesel (B100), and biodiesel blend in Gasoil (B50 and B20), were within the range of values set by the international standards specifications of diesel and biodiesel (American Society of Testing Materials and European Standard). Thus, these three produced biodiesels (B100, B50 and B20) from the Congolese Afzelia bella seeds oil could be used as a substitute for diesel without damaging the engine.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
期刊最新文献
Synthesis of Novel Perovskite-organic Hybrid Materials for High-efficiency Photovoltaic Devices Study on Micro Structural Properties of Alkali - Doped SiO2 Melt Using Molecular Dynamics Simulation Exploration of Antioxidant, Antibacterial, and Alpha-glucosidase Inhibition Potential of Cirsium verutum (D. Don) Spreng Extracts: In vitro and in silico Approach Biodegradation of Spent Oil in Soil Using Citrullus Colocynthis Peels and Other Plant Wastes Biodegradable Nypa fruticans (Nipa) Starch-PVA Biocomposite Films for Food Packaging
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1