BAMO-r-GAP共聚物/N100/IPDI固化体系粘结膜性能研究

Yibo Zhao, Yun-jun Luo, Chi Zhang
{"title":"BAMO-r-GAP共聚物/N100/IPDI固化体系粘结膜性能研究","authors":"Yibo Zhao, Yun-jun Luo, Chi Zhang","doi":"10.3969/J.ISSN.1006-9941.2013.01.015","DOIUrl":null,"url":null,"abstract":"The binder film of 3, 3-bis(azidomethy) oxetane-r-(glycidyl azide)(BAMO-r-GAP) copolymer/N100/IPDI system was synthesized using BAMO-r-GAP copolymer as pre-polymer, N100 and IPDI as curing agent and BDO as chain extended agent. The Fourier transform infrared(FT-IR) spectrometer, differential scanning calorimetry(DSC) and thermogravimetry-derivative thermogravimetry(TG-DTG) were used to characterize the binder film, and the mechanical properties was also measured. Results show that the tensile strength of the binder film is raised to 0.87 MPa, and the breaking elongation is above 106%. The glass transition temperature (Tg) of the binder film is about -50°C and the thermal decomposition starts at 217.0°C, which means the binder film has good thermal stability.","PeriodicalId":35753,"journal":{"name":"Hanneng Cailiao/Chinese Journal of Energetic Materials","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2013-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Performances of the binder film of BAMO-r-GAP copolymer/N100/IPDI curing system\",\"authors\":\"Yibo Zhao, Yun-jun Luo, Chi Zhang\",\"doi\":\"10.3969/J.ISSN.1006-9941.2013.01.015\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The binder film of 3, 3-bis(azidomethy) oxetane-r-(glycidyl azide)(BAMO-r-GAP) copolymer/N100/IPDI system was synthesized using BAMO-r-GAP copolymer as pre-polymer, N100 and IPDI as curing agent and BDO as chain extended agent. The Fourier transform infrared(FT-IR) spectrometer, differential scanning calorimetry(DSC) and thermogravimetry-derivative thermogravimetry(TG-DTG) were used to characterize the binder film, and the mechanical properties was also measured. Results show that the tensile strength of the binder film is raised to 0.87 MPa, and the breaking elongation is above 106%. The glass transition temperature (Tg) of the binder film is about -50°C and the thermal decomposition starts at 217.0°C, which means the binder film has good thermal stability.\",\"PeriodicalId\":35753,\"journal\":{\"name\":\"Hanneng Cailiao/Chinese Journal of Energetic Materials\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2013-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Hanneng Cailiao/Chinese Journal of Energetic Materials\",\"FirstCategoryId\":\"1087\",\"ListUrlMain\":\"https://doi.org/10.3969/J.ISSN.1006-9941.2013.01.015\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q3\",\"JCRName\":\"Engineering\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Hanneng Cailiao/Chinese Journal of Energetic Materials","FirstCategoryId":"1087","ListUrlMain":"https://doi.org/10.3969/J.ISSN.1006-9941.2013.01.015","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"Engineering","Score":null,"Total":0}
引用次数: 0

摘要

以BAMO-r-GAP共聚物为预聚体,N100和IPDI为固化剂,BDO为扩链剂,合成了3,3 -双(叠氮氧基)氧烷-r-(叠氮甘油酯)(BAMO-r-GAP)共聚物/N100/IPDI体系的粘结膜。采用傅里叶变换红外光谱仪(FT-IR)、差示扫描量热仪(DSC)和热重-导数热重仪(TG-DTG)对粘结膜进行表征,并对其力学性能进行了测试。结果表明:粘结膜的抗拉强度提高到0.87 MPa,断裂伸长率达到106%以上。粘结膜的玻璃化转变温度(Tg)约为-50℃,热分解开始于217.0℃,说明粘结膜具有良好的热稳定性。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
Performances of the binder film of BAMO-r-GAP copolymer/N100/IPDI curing system
The binder film of 3, 3-bis(azidomethy) oxetane-r-(glycidyl azide)(BAMO-r-GAP) copolymer/N100/IPDI system was synthesized using BAMO-r-GAP copolymer as pre-polymer, N100 and IPDI as curing agent and BDO as chain extended agent. The Fourier transform infrared(FT-IR) spectrometer, differential scanning calorimetry(DSC) and thermogravimetry-derivative thermogravimetry(TG-DTG) were used to characterize the binder film, and the mechanical properties was also measured. Results show that the tensile strength of the binder film is raised to 0.87 MPa, and the breaking elongation is above 106%. The glass transition temperature (Tg) of the binder film is about -50°C and the thermal decomposition starts at 217.0°C, which means the binder film has good thermal stability.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
Hanneng Cailiao/Chinese Journal of Energetic Materials
Hanneng Cailiao/Chinese Journal of Energetic Materials Engineering-Industrial and Manufacturing Engineering
CiteScore
1.90
自引率
0.00%
发文量
4271
期刊介绍: Chinese Journal of Energetic Materials is a vital forum for the exchange of science and technology in energetic materials, and information on - Propellants - Explosives - Pyrotechnics - Ignition, combustion and detonation
期刊最新文献
FOX-7在H 2 O/DMF溶剂中的结晶形貌预测 β型氘代奥克托今(β-HMX-d 8 )的合成 颠覆性含能材料——高风险/高回报的远期战略性基础材料 3,4-二硝基吡唑与六硝基六氮杂异伍兹烷分子间相互作用的理论研究 5,10-双(偕二硝基甲基)-呋咱并[3,4-e]双([1,2,4]三唑并)[4,3-a:3′,4′-c]吡嗪及其含能离子化合物的合成与性能
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1