纳米赤铁矿从银靶中分离109Cd

M. Sadeghi, H. Karami, P. Sarabandi, M. Mirzaee
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引用次数: 7

摘要

摘要以15mev质子辐照电镀靶,利用回旋加速器vianatAg(p, n) 109Cd反应制备了109Cd。所得收率为70 kBq/μA h。采用固相化学反应法制备纳米赤铁矿作为吸附剂进行分离。考察了pH、吸附剂浓度等参数对萃取效率的影响。采用x射线衍射(XRD)和扫描电镜(SEM)研究了纳米颗粒的相形态、纳米结构和尺寸。采用ICP-AES和HPGe探测器γ -能谱法分别测定了109Cd的化学纯度和放射性同位素纯度。
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Separation of 109Cd from silver targets by nanohematite
Abstract 109Cd was produced at a cyclotron vianatAg(p, n) 109Cd reaction by irradiation of an electroplated target with 15 MeV protons. The obtained yield was 70 kBq/μA h. The separation was performed using hematite nano-particles as sorbent which were synthesized by a solid-state chemical reaction method. The effect of different parameters, such as pH and the sorbent concentration, on extraction efficiency were investigated. The phase morphology, nanostructure and size of nano-particles were studied by X-ray diffraction (XRD) and scanning electron microscopy (SEM). The chemical and radionuclidic purity of 109Cd was determined by ICP-AES and HPGe detector gamma-ray spectrometry, respectively.
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