电流应力法合成不同形貌纳米SnO2的新方法

IF 0.6 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY 稀有金属材料与工程 Pub Date : 2018-09-01 DOI:10.1016/S1875-5372(18)30203-0
Li Wangyun, Cao Shanshan, Zhang Xinping
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引用次数: 4

摘要

利用高密度电流对两导体(铜或镍)之间由高锡含量合金组成的线状接头试样施加电流,采用一种新颖、快速、简便的方法合成了纳米氧化锡(SnO2)。制备的SnO2具有树枝状、松叶状、草状和球团状等多种形貌,并通过扫描电镜、能量色散x射线光谱和拉曼光谱证实其具有四方金红石结构。本研究不仅为制备各种形态的SnO2提供了一种简便而新颖的方法,而且为制备其他功能氧化物材料提供了一种鼓舞人心的实用思路和技术可能性。
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Novel and Facile Synthesis of Nano SnO2 with Various Morphologies by Electric Current Stressing

Nano tin oxide (SnO2) was synthesized by a novel, fast and facile approach through applying electric current of high density to a line-type joint specimen consisting of a high tin-content alloy between two pieces of conductor (copper or nickel). The fabricated SnO2 shows various morphologies, such as branch-like, pine-leaf-like, grass-like and batting-like, and has the tetragonal rutile structure confirmed by scanning electron microscopy, energy dispersive X-ray spectroscope and Raman spectrum. The present work has not only offered a facile and novel method for fabricating SnO2 of various morphologies, but also provided an inspiriting yet practical idea as well as technical possibilities for preparation of other functional oxide materials.

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来源期刊
稀有金属材料与工程
稀有金属材料与工程 工程技术-材料科学:综合
CiteScore
1.30
自引率
57.10%
发文量
17973
审稿时长
4.2 months
期刊介绍:
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