D. Mondieig, P. Négrier, J. Leger, S. Massip, B. Benali, C. Jermoumi, B. Lakhrissi
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引用次数: 0
摘要
在293 K下测定了2- s-(6′-脱氧-1′，2′:3′，4′-二o -异丙基-a- d -半乳吡喃-6′-基硫代)-3-甲基喹啉(C21H26N2O5S)的单晶结构，并在3634次反射下将其细化为R = 0.0373。该晶体为正交晶型，P212121, Z = 4。单元尺寸为:a = 11.0592(9) a, b = 11.3500(7) a, c = 16.9656(10) a, V = 2129.6(3)A3。分子由C-H***N氢键堆叠。
Crystal Structure of 2-S-(6′-Deoxy-1′,2′:3′,4′-di-O-isopropylidene-α- D -galactopyranos-6′-ylthio)-3-methylquinoxaline
The single-crystal structure of 2-S-(6′-deoxy-1′,2′:3′,4′-di-O-isopropylidene-a-D-galacto pyranos-6′-ylthio)-3-methylquinoxaline (C21H26N2O5S) was determined at 293 K and refined to R = 0.0373 for 3634 observed reflections. This crystal is orthorhombic, P212121 with Z = 4. The unit-cell dimensions are: a = 11.0592(9)A, b = 11.3500(7)A, c = 16.9656(10)A and V = 2129.6(3)A3. Molecules are stacked with C-H***N hydrogen bonds.
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