滇滇滇地生部分的化学成分

Baoping Zhou, Chunlei Zhang, Xiaoqing Zou, Jian Xu, Yan Li, Xichun Li, Chengzhi Chai, Zhengyu Cao
{"title":"滇滇滇地生部分的化学成分","authors":"Baoping Zhou, Chunlei Zhang, Xiaoqing Zou, Jian Xu, Yan Li, Xichun Li, Chengzhi Chai, Zhengyu Cao","doi":"10.11669/CPJ.2016.22.006","DOIUrl":null,"url":null,"abstract":"OBJECTIVE: To investigate the chemical constituents of the aerial parts of Ribes diacanthum Pall. METHODS: The compounds were isolated and purified by silica gel, Sephadex LH-20 colunm chromatography and HPLC. The structures were elucidated on the basis of spectral data and physiochemical properties. RESULTS: Nineteen compounds were isolated from 95% ethanol extracts and identified as quercetin (1), quercetin-3-O-β-D-glucopyranoside (2), quercetin-3-O-α-L-rhamnopyranoside (3), quercetin-3-O-β-D-neohesperoside (4), mearnsetin (5), myricetin-3-O-α-L-rhamnoside (6), myricetin-3-O-β-D-glucopyranoside (7), mearnsetin 3-O-β-D-glucopyranoside (8), mearnsetin 3-O-α-L-rhamnopyranoside (9), kaempferol-3-O-β-D-glucopyranoside (10), kaempferol 3-O-β-D-(2-O-α-L-rhamnopyranosyl) glucopyranoside (11), kaempferol 3-(2'', 6''-di-O-α-L-rhamnosyl)-β-D-glucoside (12), 1, 2, 4-trihydroxybenzene (13), vanillic acid (14), protocatechuic acid (15), 4-hydroxy benzoic acid (16), gallic acid (17), blumenol C glucoside (18), conocarpan (19). CONCLUSION: All the compounds are isolated from the title plant and the NMR data for 8 is reported here for the first time.","PeriodicalId":22409,"journal":{"name":"The Chinese Pharmaceutical Journal","volume":"1 1","pages":"1918-1922"},"PeriodicalIF":0.0000,"publicationDate":"2016-11-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"3","resultStr":"{\"title\":\"Chemical constituents from the aerial parts of ribes diacanthum pall\",\"authors\":\"Baoping Zhou, Chunlei Zhang, Xiaoqing Zou, Jian Xu, Yan Li, Xichun Li, Chengzhi Chai, Zhengyu Cao\",\"doi\":\"10.11669/CPJ.2016.22.006\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"OBJECTIVE: To investigate the chemical constituents of the aerial parts of Ribes diacanthum Pall. METHODS: The compounds were isolated and purified by silica gel, Sephadex LH-20 colunm chromatography and HPLC. The structures were elucidated on the basis of spectral data and physiochemical properties. RESULTS: Nineteen compounds were isolated from 95% ethanol extracts and identified as quercetin (1), quercetin-3-O-β-D-glucopyranoside (2), quercetin-3-O-α-L-rhamnopyranoside (3), quercetin-3-O-β-D-neohesperoside (4), mearnsetin (5), myricetin-3-O-α-L-rhamnoside (6), myricetin-3-O-β-D-glucopyranoside (7), mearnsetin 3-O-β-D-glucopyranoside (8), mearnsetin 3-O-α-L-rhamnopyranoside (9), kaempferol-3-O-β-D-glucopyranoside (10), kaempferol 3-O-β-D-(2-O-α-L-rhamnopyranosyl) glucopyranoside (11), kaempferol 3-(2'', 6''-di-O-α-L-rhamnosyl)-β-D-glucoside (12), 1, 2, 4-trihydroxybenzene (13), vanillic acid (14), protocatechuic acid (15), 4-hydroxy benzoic acid (16), gallic acid (17), blumenol C glucoside (18), conocarpan (19). CONCLUSION: All the compounds are isolated from the title plant and the NMR data for 8 is reported here for the first time.\",\"PeriodicalId\":22409,\"journal\":{\"name\":\"The Chinese Pharmaceutical Journal\",\"volume\":\"1 1\",\"pages\":\"1918-1922\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2016-11-22\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"3\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"The Chinese Pharmaceutical Journal\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.11669/CPJ.2016.22.006\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"The Chinese Pharmaceutical Journal","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.11669/CPJ.2016.22.006","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 3

摘要

目的:研究白刺地上部的化学成分。方法:采用硅胶、Sephadex LH-20柱层析和高效液相色谱法对化合物进行分离纯化。根据光谱数据和理化性质对其结构进行了鉴定。结果:19化合物- 95%乙醇提取物中分离鉴定为槲皮素(1)quercetin-3-O -β-D-glucopyranoside (2), quercetin-3-O -α-L-rhamnopyranoside (3), quercetin-3-O -β-D-neohesperoside (4), mearnsetin (5), myricetin-3-O -α-L-rhamnoside (6), myricetin-3-O -β-D-glucopyranoside (7), mearnsetin 3 -β-D-glucopyranoside (8), mearnsetin 3点-α-L-rhamnopyranoside (9), kaempferol-3-O -β-D-glucopyranoside(10)、山柰酚3 -β- d - (2 o -α-L-rhamnopyranosyl)吡喃葡萄糖苷(11),山奈酚3-(2′,6′-二- o -α- l -鼠李糖基)-β- d -葡萄糖苷(12)、1,2,4 -三羟基苯(13)、香草酸(14)、原儿茶酸(15)、4-羟基苯甲酸(16)、没食子酸(17)、蓝薄荷醇C -葡萄糖苷(18)、康康康(19)。结论:所有化合物均从该植物中分离得到,其中8个化合物的NMR数据为首次报道。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
Chemical constituents from the aerial parts of ribes diacanthum pall
OBJECTIVE: To investigate the chemical constituents of the aerial parts of Ribes diacanthum Pall. METHODS: The compounds were isolated and purified by silica gel, Sephadex LH-20 colunm chromatography and HPLC. The structures were elucidated on the basis of spectral data and physiochemical properties. RESULTS: Nineteen compounds were isolated from 95% ethanol extracts and identified as quercetin (1), quercetin-3-O-β-D-glucopyranoside (2), quercetin-3-O-α-L-rhamnopyranoside (3), quercetin-3-O-β-D-neohesperoside (4), mearnsetin (5), myricetin-3-O-α-L-rhamnoside (6), myricetin-3-O-β-D-glucopyranoside (7), mearnsetin 3-O-β-D-glucopyranoside (8), mearnsetin 3-O-α-L-rhamnopyranoside (9), kaempferol-3-O-β-D-glucopyranoside (10), kaempferol 3-O-β-D-(2-O-α-L-rhamnopyranosyl) glucopyranoside (11), kaempferol 3-(2'', 6''-di-O-α-L-rhamnosyl)-β-D-glucoside (12), 1, 2, 4-trihydroxybenzene (13), vanillic acid (14), protocatechuic acid (15), 4-hydroxy benzoic acid (16), gallic acid (17), blumenol C glucoside (18), conocarpan (19). CONCLUSION: All the compounds are isolated from the title plant and the NMR data for 8 is reported here for the first time.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
期刊最新文献
Research Progress of Pharmacokinetic Interactions between Lopinavir/Ritonavir and Statins Results and Discussion on National Vaccine Proficiency Testing Schemes in 2020 Case Study of Icotinib on The Impact of Domestic Innovative Drugs Timely Covered by Medical Insurance Evaluation of α-Interferon Applied in COVID-19 Therapy Regimen Detection and Analysis of Safety Signals of Chloroquine Based Upon FDA Adverse Event Database
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1