燃料油中总氮测定方法的建立

Jpi Sub-comm. Testing Method for Nitrogen
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引用次数: 0

摘要

根据日本石油协会的要求,日本石油研究所研究了测定燃料油中总氮的方法。本报告描述了小组委员会为建立石油产品中氮含量的测试方法和为编写JIS方法草案而组织的活动。建立了适用于含氮量大于0.01%样品的宏定氮法、微定氮法、自动杜马滴定法和微库仑滴定法。此外,还设计了一种独特的库仑法测定多种剩余油中总氮的方法。
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Establishment of Test Methods for Determination of Total Nitrogen in Fuel Oil
The Japan Petroleum Institute has investigated means for determination of total nitrogen in fuel oils as requested by the Petroleum Association of Japan.This report describes the activity of the subcommittee organized for the establishment of testing methods for nitrogen content in petroleum products and for preparation of a draft for JIS method.The committee has established four methods, macro-Kjeldahl, micro-Kjeldahl, automated Dumas, and microcoulometric titrating which are applicable to the samples containing more than 0.01%N. In addition, an unique technique for coulometrical determination of total nitrogen in many residual oils has been devised.
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