电化学法制备石榴皮提取物和壳聚糖-银纳米颗粒及其抑菌活性。

A. Sarhan, M. Hamid, Sabrien A. Omar, R. Hanie
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引用次数: 0

摘要

本文研究了壳聚糖-石榴皮提取物和纳米银粒子(Cs-PPE-AgNPs)的电化学-紫外辐照还原法制备。采用紫外-可见光谱、傅里叶变换红外光谱(FTIR)、x射线衍射(XRD)、差热分析(DTA)、扫描电镜(SEM)、膨胀和热重分析(TGA)对银纳米颗粒的形成进行表征。所得纳米颗粒平均粒径为34.6 nm。紫外光谱在405nm处出现新峰,表明AgNPs粒子形成。Cs-PPE和Cs-PPE- agnps对大肠杆菌和金黄色葡萄球菌也有较高的抑菌活性。
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Preparation, Characterization and Antibacterial Activity of Pomegranate Peel Extract and Chitosan-Silver Nanoparticles Using Electrochemical Method.
The present work involves the development of chitosan-pomegranate peel extract and silver nanoparticles (Cs-PPE-AgNPs) using electrochemical process followed by UV irradiation reduction. Formation of silver nanoparticles characterize by UV–vis spectroscopy, Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), differential thermal analysis (DTA), SEM, Swelling and thermal gravimetric analysis (TGA). The obtain nanoparticles average size was 34.6 nm. UV Spectroscopy show new peak at 405nm indicate the formation of AgNPs particles. Cs-PPE and Cs-PPE-AgNPs also demon started a relativity high antibacterial against Escherichia coli and Staphylococcus aureus bacteria.
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