磷酸氢二钾法制备大麻纤维活性炭的工艺优化及其在储热系统中的应用

L. Natrayan, S. Kaliappan, S. Subramanian, Pravin P. Patil, S. Sekar, Y. Rao, Melkamu Beyene Bayu
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摘要

活性炭纤维(ACF)与许多其他商业化的储热方法相比具有显著的优势,被认为是吸附剂用途中最好的生物吸附剂之一。如果正确制作,它是一种杰出的介孔轻质材料,具有微孔,在大多数情况下,没有微孔。ACF较高的容重和较大的动态容量证明了其在吸附剂技术中的应用价值。本研究的主要目标是从有机大麻纤维中制备活性炭纤维。选择了以下参数:(1)活化温度,(2)活化时间,(3)炭化温度,(4)活化成分%age,(5)活化温度速度,共4个级别来达到目的。采用田口优化技术对吸附剂的性能进行优化。目前的研究使用了L16正交阵列来实现这一改进。根据先前的Taguchi,最佳条件是300°C燃烧,以22.5% w / v的K2HPO4溶液受精,在800°C下以20°C/min活化3小时。温度活化率为23.35%,碳酸化温度为10.14%,增产时间为8.82%,H3PO4浓度为2.94%。结果表明,活化温度和活化速率是本研究实现最佳吸附能力的关键因素。
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Optimization of Activated Carbon Fiber Preparation from Hemp Fiber through Dipotassium Hydrogen Phosphate for Application of Thermal Storage System
With significant benefits over many other commercialised thermal storage methods, activated carbon fiber (ACF) is believed to be among the finest biosorbents for adsorbent purposes. If correctly made, it is an outstanding mesoporous lightweight material with micropores and, in most cases, no micropores. ACF’s higher bulk densities and great dynamic capacity demonstrate its value and are used in adsorbent technologies. The present study’s primary goal is to create active carbon fiber from organic hemp fiber. The following parameters were selected: (i) activating temperatures, (ii) activating timing, (iii) carbonization temperature, (iv) activating ingredient %ages, and (v) speed of activation temperature, all with four levels to achieve the goal. Taguchi optimization techniques were used to optimize the adsorbent characteristics. The current study used an L16 orthogonal array to accomplish that improvement. According to the previous Taguchi, the optimal conditions were 300°C combustions, insemination with 22.5% w / v K2HPO4 solution, and activating at 800°C for 3 hours at 20°C/min. The greatest contribution is 54.75%, followed by the rate of temperature activation at 23.35%, carbonated temperature at 10.14%, duration of stimulation at 8.82%, and H3PO4 concentrations at 2.94%. The results show that the activation temperature and rate of the temperature of activations are the essential elements in the current study’s accomplishment of the best adsorption capacities.
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