填料含量对 CAD/CAM 树脂牙冠粘接强度的影响:新型树脂底漆与传统硅烷剂的对比。

IF 4.3 3区 材料科学 Q1 ENGINEERING, ELECTRICAL & ELECTRONIC ACS Applied Electronic Materials Pub Date : 2024-04-08 Epub Date: 2023-06-07 DOI:10.2186/jpr.JPR_D_22_00301
Ryosuke Hagino, Atsushi Mine, Mariko Aoki-Matsumoto, Jiro Miura, Masahiro Yumitate, Shintaro Ban, Masaya Ishida, Munechika Takaishi, Bart Van Meerbeek, Hirofumi Yatani, Shoichi Ishigaki
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引用次数: 0

摘要

目的 本研究旨在评估含有甲基丙烯酸甲酯(MMA)和硅烷剂的树脂底漆对三种不同填料含量的间接树脂复合材料砌块粘接效果的影响。方法 对一种市售的计算机辅助设计/计算机辅助制造(CAD/CAM)树脂复合材料砌块和两种不同填料含量的实验性树脂复合材料砌块进行氧化铝喷砂,并进行两种表面处理(底漆和硅烷剂)。砌筑树脂胶结物,并在贮水 24 小时、1 个月或 3 个月后测量微拉伸粘接强度(μTBS)(每组 n = 24)。结果 只有在 F0(填料含量为 0 wt%)组中,底漆处理组的粘结强度明显高于硅烷组(P < 0.001)。在底漆组中,F0 和 F41(填料含量为 41 wt%)组的粘接强度明显高于 F82(填料含量为 82 wt%)组(P < 0.001)。相比之下,在硅烷组中,F41 组的粘接强度明显高于 F0 和 F82 组(P < 0.001),F82 组的粘接强度明显高于 F0 组(P < 0.001)。扫描电子显微镜显示,与硅烷组相比,底漆组断裂面上的基质树脂部分被破坏,且界面表面不平整。
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Effect of filler contents on the bond strength of CAD/CAM resin crowns: New resin primer versus conventional silane agents.

Purpose This study aims to evaluate the effects of resin primers containing methyl methacrylate (MMA) and silane agent on the bonding effectiveness of indirect resin composite blocks with three different filler contents.Methods A commercially available computer-aided design/computer-aided manufacturing (CAD/CAM) resin composite block and two experimental resin composite blocks with different filler contents were alumina-blasted and two surface treatments (primer and silane agent) were applied. The resin cement was built up, and the micro-tensile bond strength (μTBS) was measured after 24 hours, 1 month or 3 months of water storage (n = 24 per group). The fracture surfaces after μTBS measurements and resin block/cement interface were observed by scanning electron microscopy (SEM).Results The primer treatment group showed a significantly higher bond strength than the silane group only in F0 (filler content 0 wt%) group (P < 0.001). In the primer group, F0 and F41 (filler content 41 wt%) groups showed significantly higher bond strengths than F82 (filler content 82 wt%) group (P < 0.001). In contrast, in the silane group, F41 group showed significantly higher bond strength than F0 and F82 groups (P < 0.001), and F82 group showed significantly higher bond strength than F0 group (P < 0.001). SEM revealed that the matrix resin was partially destroyed on the fracture surface of the primer group, and an uneven interface surface was observed compared with that of the silane group.Conclusions MMA-containing primers showed higher bonding effectiveness to CAD/CAM resin composite blocks than the silane treatment.

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4.30%
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567
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