Preparation and Characterization of NiCoFerrite Nanoparticles by Thermal Method

M. Naseri, E. Saion, H. A. Ahangar
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Abstract

The NiCoFerrite nanoparticle has been prepared using thermal method. Polyvinyl pyrrolidon (PVP) was used as a reducing agent due to its reducing effect on agglomeration of particles. The characterization studies such as X-ray diffraction (XRD) and transmission electron microscopy (TEM) have been done for explore the particles size. By Scherer"s equation the average particles size has been estimated that support TEM results. An increasing in particles size was observed with increasing calcinations temperature. FTIR confirmed the presence of metal oxide.
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镍铁氧体纳米颗粒的热法制备与表征
采用热法制备了镍铁氧体纳米颗粒。采用聚乙烯吡咯烷酮(PVP)作为还原剂,以减少颗粒团聚。通过x射线衍射(XRD)和透射电子显微镜(TEM)等表征研究了颗粒的大小。根据Scherer方程估计出了与TEM结果相符的平均粒径。随着煅烧温度的升高,颗粒尺寸逐渐增大。红外光谱证实了金属氧化物的存在。
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