Titanium - carbon multilayer nanostructures obtained by thermionic vacuum arc method

V. Ciupină, C. Lungu, E. Vasile, G. Prodan, C. Porosnicu, R. Vlǎdoiu, A. Mandeş, V. Dinca, V. Nicolescu, M. Prodan, R. Manu
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引用次数: 2

Abstract

Titanium-Carbon (Ti-C) multilayer nanostructures were deposed by Thermionic Vacuum Arc (TVA) technology. The layers consisting of about 100 nm Carbon base layer and seven 40 nm alternatively Ti and C layers were deposed on Silicon substrates. The thickness of such a multilayer structure was up to 500 nm. On the other hand, in order to obtain Ti-C multilayer structures with various Ti content, a 20nm thick C layer was first deposed on Si substrate and then seven successively Ti-C layers (Ti and C simultaneously deposed), each of these having a thickness of up to 40 nm were deposed. To perform the successively Ti-C layers with various Ti content were changed the discharge parameters for C and Ti plasma sources to obtain the desirable Ti atomic concentration To characterize microstructure properties of as prepared C-Ti multilayer structures were used Rutherford Backscattering Spectrometry (RBS), Electron microscopy techniques (TEM, STEM), Raman Spectroscopy and electrical measurements.Titanium-Carbon (Ti-C) multilayer nanostructures were deposed by Thermionic Vacuum Arc (TVA) technology. The layers consisting of about 100 nm Carbon base layer and seven 40 nm alternatively Ti and C layers were deposed on Silicon substrates. The thickness of such a multilayer structure was up to 500 nm. On the other hand, in order to obtain Ti-C multilayer structures with various Ti content, a 20nm thick C layer was first deposed on Si substrate and then seven successively Ti-C layers (Ti and C simultaneously deposed), each of these having a thickness of up to 40 nm were deposed. To perform the successively Ti-C layers with various Ti content were changed the discharge parameters for C and Ti plasma sources to obtain the desirable Ti atomic concentration To characterize microstructure properties of as prepared C-Ti multilayer structures were used Rutherford Backscattering Spectrometry (RBS), Electron microscopy techniques (TEM, STEM), Raman Spectroscopy and electrical measurements.
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热离子真空电弧法制备钛碳多层纳米结构
采用热离子真空电弧(TVA)技术沉积钛碳(Ti-C)多层纳米结构。在硅衬底上沉积了约100 nm的碳基层和7个40 nm的Ti和C交替层。该多层结构的厚度可达500 nm。另一方面,为了获得不同Ti含量的Ti-C多层结构,首先在Si衬底上沉积20nm厚的C层,然后连续沉积7层Ti-C层(Ti和C同时沉积),每层厚度可达40nm。为了连续制备不同Ti含量的Ti-C层,改变了C和Ti等离子体源的放电参数,以获得所需的Ti原子浓度。采用卢瑟福后向散射光谱(RBS)、电子显微镜技术(TEM、STEM)、拉曼光谱和电学测量等方法表征了制备的C-Ti多层结构的微观结构特性。采用热离子真空电弧(TVA)技术沉积钛碳(Ti-C)多层纳米结构。在硅衬底上沉积了约100 nm的碳基层和7个40 nm的Ti和C交替层。该多层结构的厚度可达500 nm。另一方面,为了获得不同Ti含量的Ti-C多层结构,首先在Si衬底上沉积20nm厚的C层,然后连续沉积7层Ti-C层(Ti和C同时沉积),每层厚度可达40nm。为了连续制备不同Ti含量的Ti-C层,改变了C和Ti等离子体源的放电参数,以获得所需的Ti原子浓度。采用卢瑟福后向散射光谱(RBS)、电子显微镜技术(TEM、STEM)、拉曼光谱和电学测量等方法表征了制备的C-Ti多层结构的微观结构特性。
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