Structural phase transformation of FePt nanoparticles by ion irradiation

B. Rellinghaus, O. Dmitrieva, M. Liedke, J. Fassbender
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Abstract

In the present study, post-deposition 5 keV He irradiation has been performed on such gas phase prepared FePt nanoparticles. Structural characterization of the samples is carried out by means of high resolution transmission electron microscopy (HRTEM). The power spectra obtained by Fourier transform of the original images clearly show that the particles are multiply twinned and of icosahedral structure but after irradiation, the particles are now of single crystal fcc structure and their mean diameter is reduced. This size reduction is ascribed to irradiation induced sputtering of the particles.
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离子辐照下FePt纳米颗粒的结构相变
在本研究中,对这种气相制备的FePt纳米颗粒进行了沉积后的5 keV He辐照。通过高分辨率透射电子显微镜(HRTEM)对样品进行结构表征。对原始图像进行傅里叶变换得到的功率谱清楚地表明,粒子是多重孪晶和二十面体结构,但经过辐照后,粒子变成单晶fcc结构,平均直径减小。这种尺寸减小归因于辐照引起的颗粒溅射。
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