Antimicrobial effect of nylon fiber immersed with nano-silver

A. Haryono, S. B. Harmami, D. Sondari
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Abstract

The development of new products based on the immobilization of nanoparticles on fibers has recently received a growing interest from both the academic and industrial sectors. A wide range of nanoparticles and nano-structures can be immobilized on fibers, which brings new properties to the final product. In the present work, silver nanoparticle was immobilized on nylon fibers by immersed deposition method as an antimicrobial agent. Silver colloid was produced by chemical reduction of silver salt (silver nitrate) solution, in the presence of sodium citrate. Synthesis of silver colloid was carried out by using chemical reduction method at temperature of 95 and 100°C. The mixture was heated until color changed into pale yellow. UV-Vis spectrometry indicated formation of silver nanoparticles. UV-Vis analysis was reported that the absorption spectrum of silver nanoparticles showed a maximum between 420 and 450 nm. Characterization of silver nanoparticles was conducted using Fourier Transformed Infra Red (FTIR) spectroscopy, UV-Vis spectroscopy, particle size analyzer (PSA), and scanning electron microscope (SEM). It was found that silver nanoparticles forms aggregates on the surface of fiber, during deposition process. The size of aggregates varied from 19.9 ± 4.8 nm to 49.5 ± 12.5 nm. To evaluate the antimicrobial effects against microorganisms, we used representative microorganisms S. aureus. Silver nanoparticles showed antimicrobial activity reducing bacterial growth.
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纳米银浸渍尼龙纤维的抗菌效果
基于纳米颗粒固定在纤维上的新产品的开发最近受到了学术界和工业界越来越大的兴趣。广泛的纳米颗粒和纳米结构可以固定在纤维上,从而给最终产品带来新的性能。本研究采用浸没沉淀法将纳米银作为抗菌剂固定在尼龙纤维上。在柠檬酸钠存在下,用硝酸银溶液化学还原法制备银胶体。在95℃和100℃的温度下,采用化学还原法制备银胶体。把混合物加热,直到颜色变成淡黄色。紫外可见光谱分析表明银纳米颗粒的形成。紫外可见光谱分析表明,纳米银的吸收光谱在420 ~ 450 nm之间有最大值。利用傅里叶变换红外光谱(FTIR)、紫外可见光谱(UV-Vis)、粒径分析仪(PSA)和扫描电镜(SEM)对纳米银进行了表征。在沉积过程中,纳米银颗粒在纤维表面形成聚集体。聚集体的大小从19.9±4.8 nm到49.5±12.5 nm不等。为了评价其对微生物的抗菌作用,我们选用了具有代表性的金黄色葡萄球菌。银纳米颗粒具有抑制细菌生长的抗菌活性。
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