Spherical to polyhedral Pt nanocrystal formation assisted with methylamine

M. Ooi, A. Aziz
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引用次数: 1

Abstract

Nanocrystalline Pt particles synthesized by solvothermal technique assisted with methylamine were investigated. The effect of different amounts of methylamine on the formation of Pt nanocrystal were characterized and elaborated. Small and spherical - like particles were observed for Pt synthesized under the low amount (0.10 mL) of methylamine whilst, concave polyhedral Pt nanocrystal with high - index {411} facets were observed for Pt synthesized under high amount (0.20 mL) of methylamine. The synthesized concave Pt nanocrystal exhibit high absorption peak at 215 nm corresponding to colloidal Pt. The synthesized concave polyhedral structures could be used as a potential catalyst in fuel cells application.
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甲胺辅助形成球形到多面体的铂纳米晶体
研究了甲胺辅助溶剂热法制备纳米晶铂颗粒。研究了不同量的甲胺对铂纳米晶形成的影响。在低剂量(0.10 mL)甲胺条件下,合成的Pt呈小球形颗粒;在高剂量(0.20 mL)甲胺条件下,合成的Pt呈凹形多面体纳米晶体,具有高折射率{411}切面。所合成的凹形Pt纳米晶体在215 nm处具有较高的吸收峰,与胶体Pt相对应。所合成的凹形多面体结构可作为一种潜在的燃料电池催化剂应用。
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