Experimental Production of Multicomponent Crystals with M-type Hexaferrite Structure

O. Zaitseva, D. E. Zhivulin, D. Galkina
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Abstract

The experimental production of multicomponent crystals with M-type hexaferrite structure, the qualitative and quantitative composition of which reflects the formula AB 12 O 19 , where A is Ba, Pb, Sr, Ca, Zn, and B is Fe, Mn, Ni, Ti, Al, Cu, W is carried out. The resulting material of this composition in the future can provide the ability to smoothly change the frequency of ferromagnetic resonance and throughput. In this way, the properties required by electronic equipment manufacturers can be obtained. In the course of the research, have been studied the possibilities of using different methods for synthesizing experimental samples – solid-phase sintering, melting in a platinum crucible, and melting in a stainless steel crucible. According to SEM and EDX results of the obtained samples, two main types of multicomponent crystalline phases were found: hexagonal crystals having the structure of hexaferrite M-type and octahedral crystals having the structure of spinel AB 2 O 4
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m型六铁体结构多组分晶体的实验制备
实验制备了具有m型六铁素体结构的多组分晶体,其定性和定量组成反映公式ab12o19,其中A为Ba、Pb、Sr、Ca、Zn, B为Fe、Mn、Ni、Ti、Al、Cu、W。该组合物在未来可以提供平滑改变铁磁共振频率和通量的能力。通过这种方式,可以获得电子设备制造商所要求的性能。在研究过程中,研究了用不同的方法合成实验样品的可能性——固相烧结、铂坩埚熔化和不锈钢坩埚熔化。通过对样品的SEM和EDX分析,发现了两种主要的多组分晶相:具有六铁体m型结构的六方晶体和具有尖晶石AB 2o结构的八面体晶体
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