Study on Applicability of Master Curve Methodology Using Miniature C(T) Specimen to a Reactor Pressure Vessel With Low Upper Shelf Energy

K. Yoshimoto, T. Hirota, H. Sakamoto, Oshikiri Masato, K. Tsutsumi, Murakami Takeshi
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Abstract

Miniature compact tension (Mini-C(T)) specimen can be an effective tool by utilizing together with Master Curve (MC) methodology for fracture toughness evaluation of irradiated reactor pressure vessel (RPV) steels. Recently, Mini-C(T) specimen has been incorporated into the Japanese standard test method related to MC methodology, JEAC4216-2015 and several studies were found focusing on applicability of Mini-C(T) specimen to irradiated RPV materials. However, there exist some other issues to be resolved considering application to irradiated materials. One of them is violation against the limitation criteria for ductile crack growth (DCG) specified in the standards. In general, upper shelf energy (USE) of RPV materials tends to decrease as well as shift in Charpy transition temperature due to neutron irradiation embrittlement. It may cause reduction in resistance of material against DCG and this leads to the problem peculiar to low USE materials such that the limitation for DCG might be dominant rather than that for KJclimit. Therefore, it is possible to fail to obtain valid KJc data even within valid temperature range of MC methodology, i.e. −50°C ≤ T-To ≤ 50°C, for low USE materials using Mini-C(T) specimens. In this study, the RPV steel with USE lower than 68J was made simulating reduction of USE due to neutron irradiation. Fracture toughness tests were performed using Mini-C(T) specimens as well as the standard 1T-C(T) specimens. Based on the test results, the validity for DCG limitation was also evaluated for each datum by post-test observation of fracture surface. Additionally, effectiveness of added side grooves and double thickness of specimen was examined as a countermeasure for Mini-C(T) specimen.
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小型C(T)试样主曲线法在低上架能量反应堆压力容器上的适用性研究
微型紧致拉伸(Mini-C(T))试样可与主曲线(MC)方法相结合,成为评价辐照反应堆压力容器(RPV)钢断裂韧性的有效工具。最近,Mini-C(T)试样被纳入日本MC方法论相关标准试验方法JEAC4216-2015,并发现了几项关于Mini-C(T)试样对辐照RPV材料适用性的研究。然而,考虑到辐照材料的应用,还存在一些其他问题需要解决。其中之一是违反了标准中规定的延性裂纹扩展(DCG)限制准则。一般情况下,由于中子辐照脆化,RPV材料的上架能(USE)有降低和夏比转变温度偏移的趋势。它可能会导致材料对DCG的阻力降低,这导致低使用材料特有的问题,例如DCG的限制可能占主导地位,而不是KJclimit。因此,即使在MC方法的有效温度范围内(即- 50°C≤T- to≤50°C),对于使用Mini-C(T)样品的低使用材料,也可能无法获得有效的KJc数据。在本研究中,模拟中子辐照降低USE,制备了USE低于68J的RPV钢。断裂韧性试验采用Mini-C(T)试样和标准1T-C(T)试样进行。在试验结果的基础上,通过试验后对断口表面的观察,对各基准进行了DCG限限的有效性评价。此外,还考察了增加侧槽和双厚度试样作为微型c (T)试样的对策的有效性。
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