Experimental characterization of conformal hydrodynamic nanopolishing of a machined single crystal sapphire cavity

Pradeep Kumar, R. Mittal, R. Singh, S. Joshi
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Abstract

Sapphire is an important ceramic material which finds applications in fields such as temperature sensing, optics, electronics, and ceramic bearings. Polishing of sapphire has always been a difficult task for industries and research communities. Hydrodynamic polishing (HDP) is one of the prominent methods used for polishing of hard and profiled surfaces, whereas rigid tool-based methods such as diamond turning, grinding, and honing have many limitations. The HDP process involves deterministic flow of abrasive particles in the slurry between the workpiece surface and a rotating soft tool to obtain the desired surface finish. A novel experimental setup has been fabricated to realize the conformal hydrodynamic nanopolishing on single crystal sapphire cavity. In this study, the experiments were conducted to understand the effect of abrasive particle size, basicity of slurry, and change in temperature of slurry on the polishing of machined sapphire cavity. The effect of the initial surface roughness of the machined cavity on conformal hydrodynamic nanopolishing has also been investigated. A microcrack/pit-free surface has been found after the final polishing of the sapphire cavity. An improvement of 21% is found in surface finish after the final polishing using abrasive particle size of 0.06 µm. Abrasive slurry with higher basicity (pH 13) does not improve the surface finish. By heating the abrasive slurry to a temperature of 70°C–75°C, surface finish improves by ∼26% as compared to improvement of ∼ 21% at room temperature polishing.
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单晶蓝宝石腔体共形水动力纳米抛光的实验表征
蓝宝石是一种重要的陶瓷材料,在温度传感、光学、电子和陶瓷轴承等领域都有应用。蓝宝石的抛光一直是工业界和研究界的一项艰巨任务。流体动力抛光(HDP)是用于硬表面和异形表面抛光的主要方法之一,而基于刚性工具的方法,如金刚石车削,磨削和珩磨有许多局限性。HDP工艺涉及在工件表面和旋转软工具之间的料浆中磨料颗粒的确定性流动,以获得所需的表面光洁度。为实现蓝宝石单晶腔体的保形水动力纳米抛光,建立了一种新的实验装置。本研究通过实验了解磨料粒度、料浆碱度、料浆温度变化对加工后蓝宝石腔体抛光的影响。研究了加工腔体初始表面粗糙度对共形水动力纳米抛光的影响。在对蓝宝石腔体进行最后抛光后,发现了一个微裂纹/无凹坑的表面。使用0.06 μ m磨料粒度进行最终抛光后,表面光洁度提高21%。较高碱度(pH 13)的磨料浆不能改善表面光洁度。通过将磨料浆加热到70°C - 75°C的温度,表面光洁度提高了~ 26%,而室温抛光的表面光洁度提高了~ 21%。
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