Microstructural Characterization of Micro-Textured Titanium Surfaces

W. Soboyejo, C. Mercer, S. Allameh, B. Nemetski, N. Marcantonio, J. Ricci
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Abstract

This paper presents the results of a multi-scale microstructural characterization of micro-textured Ti-6Al-4V surfaces that are used in biomedical implants. The hierarchies of substructural and microstructural features associated with laser micro-texturing, polishing and surface blasting with alumina pellets are elucidated via atomic force microscopy (AFM), transmission electron microscopy (TEM), scanning electron microscopy (SEM) and optical microscopy (OM). The nano-scale roughness profiles associated with the different surface textures are elucidated via AFM. Sub-micron precipitates and dislocation substructures associated with wrought processing and laser processing are revealed by TEM. Micro- and meso-scale images of the groove structures are then discussed using OM and SEM. The implications of the results are discussed for the optimization of laser processing schemes for the fabrication of micro-textured surfaces that will facilitate the self organization of proteins, and the attachment of mammalian cells to the Ti-6Al-4V surfaces in biomedical implants.
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微织构钛表面的微观结构表征
本文介绍了用于生物医学植入物的微纹理Ti-6Al-4V表面的多尺度微观结构表征结果。通过原子力显微镜(AFM)、透射电子显微镜(TEM)、扫描电子显微镜(SEM)和光学显微镜(OM)分析了氧化铝颗粒激光微纹理、抛光和表面爆破的亚结构和微观结构特征。通过原子力显微镜分析了不同表面结构的纳米尺度粗糙度分布。透射电镜观察了变形加工和激光加工的亚微米析出物和位错亚结构。然后用OM和SEM对沟槽结构的微观和中尺度图像进行了讨论。研究结果对优化激光加工方案的意义进行了讨论,以制造微纹理表面,促进蛋白质的自组织,以及哺乳动物细胞在生物医学植入物Ti-6Al-4V表面的附着。
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