Using Individual Spectra Simulation for the Study of Pole Figures Errors

T. Lychagina, D. Nikolayev, F. Wagner
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引用次数: 3

Abstract

Crystallographic texture is described by pole figures. In this paper, we continue to study experimental pole figure errors. In other words it can be named pole figure measurement errors. These errors are connected with the experimental procedure and do not depend on any further computations. In our previous works it was shown that the qualitative behaviour of pole figure measurement errors is similar to peak width determination errors. To check this conclusion a set of diffraction spectra were measured for Mg + 4.5%Al + 1%Zn sample on the spectrometer for quantitative texture analysis (SKAT) at FLNP, JINR, Dubna. Then we simulated the individual spectra and used these spectra for the pole figure extraction and the pole figure error determination. Such simulation enabled to confirm conclusions concerning the main role of the peak width determination error in the pole figure error. Additionally, we simulated individual spectra using model pole figures and extracted pole figures and pole figures errors from those spectra. For this case we also confirmed the same qualitative behaviour of pole figure measurement errors and peak width determination errors. The model pole figures were calculated on the basis of normal distributions.
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用个别光谱模拟研究极形误差
晶体结构用极形来描述。在本文中,我们继续研究实验极形误差。换句话说,它可以被命名为极形测量误差。这些误差与实验过程有关,不依赖于任何进一步的计算。在我们以前的工作中,已经证明了极形测量误差的定性行为与峰宽测定误差相似。为了验证这一结论,我们在杜布纳FLNP, JINR, Dubna的定量织构分析光谱仪(SKAT)上测量了Mg + 4.5%Al + 1%Zn样品的衍射光谱。在此基础上,对单个光谱进行模拟,并利用这些光谱进行极图提取和极图误差确定。这样的模拟可以证实峰宽测定误差在极形误差中起主要作用的结论。此外,我们利用模型极点图模拟了各个光谱,并从这些光谱中提取了极点图和极点图误差。在这种情况下,我们也证实了极形测量误差和峰宽确定误差相同的定性行为。模型极点数是根据正态分布计算的。
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