ADVANTAGES AND DISADVANTAGES OF DIFFERENT METHODS FOR STUDYING THE PHASE-STRUCTURAL STATES OF MATERIALS (A REVIEW)

Hanna Kniazieva (Postelnyk), Serhii Kniaziev, M. Tkachuk, N. Pinchuk
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Abstract

The paper provides a brief overview of the standard capabilities of X-ray techniques for studying materials with examples of modern performance of elemental and structural studies. X-ray research methods make it possible to reveal the elemental and phase-structural state. Thanks to modern software and electronic databases, the use of previously complex techniques is becoming simpler and more accessible. To illustrate the solution of specific problems, several examples of obtaining and decoding diffraction patterns and identifying the phase composition of the coating and ceramic material are given. An example of work in modern specialized software for acceleration and automation of phase identification is shown. For clarity, an example of identifying phases using electronic database cards is presented, which is still used today for manual decoding.  The practice of interaction between researchers shows that even specialists in the field of X-ray structural analysis are not always aware of modern methods of processing and decoding the obtained data. The possibilities and algorithm of action in research can be interesting for students, engineers, researchers of materials science and mechanical engineering profile. Keywords: microscopy, X-raystructural analysis, X-rayfluorescence analysis
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不同材料相结构态研究方法的优缺点(综述)
本文简要概述了x射线技术用于研究材料的标准能力,并举例说明了元素和结构研究的现代性能。x射线研究方法使揭示元素和相结构状态成为可能。由于有了现代软件和电子数据库,以前复杂的技术的使用变得更加简单和容易。为了说明具体问题的解决方法,给出了几个获得和解码衍射图以及识别涂层和陶瓷材料相组成的例子。并举例说明了在现代相位识别加速与自动化专用软件中的工作。为了清楚起见,本文给出了一个使用电子数据库卡片识别相位的例子,这种卡片至今仍用于人工解码。研究人员之间相互作用的实践表明,即使是x射线结构分析领域的专家也并不总是知道处理和解码所获得数据的现代方法。研究中行动的可能性和算法对于学生,工程师,材料科学和机械工程概况的研究人员来说是有趣的。关键词:显微镜,x射线结构分析,x射线荧光分析
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