Characterization and Microwave Absorption Properties of Lead-Free Bi0.5(Na0.80K0.20)0.5TiO3 Synthesized by Sol-Gel Method

N. Co, Bui Thi Thu Thuy, Nguyen Thi Luong, Dong Quoc Viet, Le Viet Cuong, Dang Duc Dung, Ngo Duc Quan, Tran Mau Danh, Pham Duc Thang, Bui Dinh Tu
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Abstract

Lead-free Bi0.5(Na0.80K0.20)0.5TiO3 (BNKT) particles were synthesized by using  sol-gel method. The samples were investigated by X-ray diffractometry (XRD), scanning electron microscope (SEM), energy-dispersive X-ray spectroscopy (EDX), and vibrating sample magnetometer (VSM). The absorption of microwaves of the lead-free BNKT powders is determined from the magnetic (permeability) and dielectric (permittivity) properties at the frequency range from 2 to 18 GHz. Absorption characteristics of paraffin(wax)-mixed BNKT compounds at different sample thicknesses were also investigated. The microwave absorption properties show that the maximum reflection loss is -21.72 dB (99.9%) at 13.66 GHz with a thickness of 3.2 mm. BNKT composites are thought to be used as a promising microwave absorption material.  
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溶胶-凝胶法制备无铅Bi0.5(Na0.80K0.20)0.5TiO3的表征及微波吸收性能
采用溶胶-凝胶法制备了无铅Bi0.5(Na0.80K0.20)0.5TiO3 (BNKT)颗粒。采用x射线衍射仪(XRD)、扫描电镜(SEM)、能量色散x射线能谱仪(EDX)和振动样品磁强计(VSM)对样品进行了表征。无铅BNKT粉末在2 ~ 18 GHz频率范围内的磁(导率)和介电(介电常数)特性决定了其对微波的吸收。研究了不同样品厚度下石蜡混合BNKT化合物的吸收特性。微波吸收特性表明,在13.66 GHz,厚度为3.2 mm时,最大反射损耗为-21.72 dB(99.9%)。BNKT复合材料被认为是一种很有前途的微波吸收材料。
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