The influence of dislocation and twin structures on the mechanical characteristics of Ni–Mn–Ga alloys at ultrasonic frequencies

V. V. Kaminskii, D. A. Kalganov, E. Podlesnov, A. Romanov
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Abstract

Magnetic shape memory alloys are a specific subtype of shape memory materials. The magnetic deformation phenomenon causes the high research interest in these alloys. Thus, in one of the most promising alloys based on Ni–Mn–Ga, using a magnetic field, it is possible to achieve changes in a single crystal size by up to 10 % due to the reorientation of the magnetic field in magnetic domains. The high magnetic deformation is directly related to the high mobility of twin boundaries separating two domains. In this work, the authors used a composite piezoelectric oscillator at a frequency of about 100 kHz to determine the influence of such defects as dislocations and twin boundaries on the mechanical characteristics of Ni49Mn30Ga21. The authors investigated the features of temperature dependences of internal friction in the samples before and after deformation and provided the amplitude dependences of these characteristics. In the studied single-crystal martensitic phase, the transition from the tetragonal phase to the orthorhombic phase was detected at 235 K. In the Ni–Mn–Ga tetragonal phase, the formation of new defects contributes to the more pronounced and early onset of amplitude-dependent internal friction. At lower loads, the successive stages occur associated with the processes of dislocations and twin boundaries movements inside the Cottrell clouds, dislocations and twin boundaries movement outside the Cottrell clouds, and supposedly, the slowdown of dislocations and twin boundaries movement due to their interaction. As well as internal friction, the authors studied the change in Young’s modulus. Its decrease at all temperatures is most pronounced in the samples with the defective structures. The study identified that in the orthorhombic phase, it is possible to observe the internal friction dependence on the deformation amplitude at a lower load due to an increase in the twin boundaries mobility with increasing temperature.
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超声频率下位错和孪晶组织对Ni-Mn-Ga合金力学特性的影响
磁性形状记忆合金是形状记忆材料的一个特殊子类。磁变形现象引起了这些合金的高度研究兴趣。因此,在基于Ni-Mn-Ga的最有前途的合金之一中,使用磁场,由于磁场在磁域中的重新定向,有可能实现单晶尺寸的变化高达10%。高磁变形与分离两畴的孪晶界的高迁移率直接相关。在这项工作中,作者使用频率约为100 kHz的复合压电振荡器来确定位错和孪晶边界等缺陷对Ni49Mn30Ga21力学特性的影响。作者研究了变形前后试样内摩擦的温度依赖性特征,并给出了这些特征的振幅依赖性。单晶马氏体相在235 K时由四方相转变为正交相。在Ni-Mn-Ga四方相中,新缺陷的形成导致了更明显和更早的振幅依赖内摩擦。在较低载荷下,连续阶段的发生与Cottrell云内的位错和孪晶界运动过程有关,与Cottrell云外的位错和孪晶界运动过程有关,并且由于它们的相互作用,可能会导致位错和孪晶界运动的减缓。除了内摩擦外,作者还研究了杨氏模量的变化。在具有缺陷结构的样品中,其在所有温度下的下降最为明显。研究发现,在正交相中,由于孪晶界迁移率随温度升高而增加,可以观察到在较低载荷下内摩擦与变形幅度的依赖关系。
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