Development of helium-microwave-induced plasma-atomic emission spectroscopy system with two-way spectroscopic analysis

S. Ikezawa, J. Yamamoto, T. Ueda
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引用次数: 1

Abstract

This paper reports on a helium-microwave-induced plasma-atomic emission spectroscopy (He-MIP-AES) system with two-way spectroscopic analysis that fulfills the criteria prescribed by the Ministry of Environment, Japan, for measuring the chemical components of particulate matter (PM). The He-MIP-AES system is a reconstruction of a commercial particle analyzer system. In current environmental monitoring systems, PMs are typically collected on trapping filters placed across Japan and classified as either suspended particulate matter (SPM) or PM2.5 depending on the size. The collected PMs are subsequently analyzed with automated measurement instruments such as a piezo balance and with methods such as beta ray attenuation and light scattering. While these measurement methods allow the mass concentration of PMs in the air to be obtained at hourly intervals, the chemical composition of individual particles is analyzed with time-intensive laboratory procedures. In contrast, the presented measurement system allows the chemical compositions and particle sizes to be measured simultaneously in real time.
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双向光谱分析氦-微波等离子体-原子发射光谱系统的研制
本文报道了一种具有双向光谱分析的氦-微波诱导等离子体原子发射光谱(He-MIP-AES)系统,该系统符合日本环境省规定的用于测量颗粒物(PM)化学成分的标准。He-MIP-AES系统是对商用粒子分析系统的改造。在目前的环境监测系统中,pm通常是通过放置在日本各地的捕集过滤器收集的,并根据大小将其分类为悬浮颗粒物(SPM)或PM2.5。收集到的pm随后用自动测量仪器(如压电天平)和射线衰减和光散射等方法进行分析。虽然这些测量方法可以每小时获得空气中pm的质量浓度,但单个颗粒的化学成分是通过耗时的实验室程序进行分析的。相比之下,所提出的测量系统可以同时实时测量化学成分和颗粒大小。
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