RESEARCH OF THE INFLUENCE OF THE MODE PARAMETERS OF THE WATER-VACUUM EXTRACTION PROCESS ON THE YIELD OF BIOLOGICALLY ACTIVE SUBSTANCES INONOTUS OBLIQUUS

R. Safin, S. Mukhametzyanov, A. Safina, N. Galyavetdinov, V. Gubernatorov
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Abstract

Inonotus obliquus or chaga birch mushroom has a fairly wide range of applications in the cosmetic, food and pharmaceutical industries due to the wide range of biologically active substances it contains. The analysis of foreign and domestic studies testifies to the ongoing research in the field of extraction of valuable components from chaga, however, issues of intensification of processes and the development of new methods of extraction remain topical. One of these methods is the water-vacuum extraction of chaga, which consists in alternating the stages of the process at atmospheric and reduced pressure. The aim of the study is to determine the optimal time parameters of the individual stages of the water-vacuum extraction of chaga to optimize the operating parameters of the process. The object of the study was chaga collected in forest plantations in central Russia in the spring season, and crushed to particles ranging in size from 0.1 to 1.2 mm. The experiments were carried out on a laboratory version of a vacuum extraction unit, which allows for the classical infusion and extraction of chaga at various variations in the pressure of the medium. Studies have shown that preliminary evacuation of dry raw materials and the introduction of a rarefied medium into the process of water extraction of chaga makes it possible to intensify the extraction process and has a positive effect on the yield and activity of extractive substances. It has been established that the preliminary evacuation of crushed chaga makes it possible to increase the efficiency of subsequent extraction and to increase the yield of valuable components by 15-18%. The optimal time for this stage was 5 minutes. The effective duration of the infusion step at atmospheric pressure was 30 minutes, and the subsequent evacuation is expediently carried out for 10 minutes. Based on the results of the presented work, the optimal scheme for carrying out the process of water-vacuum extraction of chaga was determined.
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水-真空萃取工艺模式参数对斜花草生物活性物质产率的影响研究
白桦蘑菇由于其含有大量的生物活性物质,在化妆品、食品和制药工业中有着相当广泛的应用。对国内外研究的分析表明,从桦茸中提取有价值成分的研究正在进行中,但强化工艺和开发新的提取方法的问题仍然是当前的热点。其中一种方法是chaga的水真空萃取,它包括在常压和减压下交替进行过程的各个阶段。研究的目的是确定chaga水真空提取各阶段的最佳时间参数,以优化该工艺的操作参数。研究对象是春季在俄罗斯中部的森林种植园收集的chaga,并将其粉碎成0.1至1.2毫米的颗粒。实验是在实验室版的真空提取装置上进行的,该装置允许在各种介质压力下进行经典的灌注和提取chaga。研究表明,在白桦茸水提过程中预先抽除干燥原料和引入稀薄介质,可以强化提取过程,并对提取物质的得率和活性产生积极影响。研究表明,对破碎的chaga进行初步抽提,可以提高后续提取的效率,使有价成分的得率提高15-18%。这个阶段的最佳时间是5分钟。常压下输液步骤的有效持续时间为30分钟,随后方便进行10分钟的疏散。在此基础上,确定了白桦茸水真空提取工艺的最佳方案。
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