OPERATIONAL CONTROL OF THE PROCESS OF PRIMARY PROCESSING OF HYDROCARBONS

Nabil Abdel Sater, Grigorov A. B.
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Abstract

The article considers the ways to solve the problem that arises during the primary processing of hydrocarbon (oil, gas condensate, etc.) raw materials and in the technical literature is called: "the fraction superposition effect". This problem is related to the use of technological equipment, including distillation columns, and can be solved by operational control and regulation of technological parameters (temperature, pressure, amount of fusion, etc.) of the process of separation of hydrocarbons into fractions. Operational control of the raw material division into fractions should be based on a system that includes a unit of operational control of technological parameters (quality indicators of distillate fractions) and a correction unit that allows immediate adjustment of parameters to the required level to ensure a certain quality of products. Primary information on the qualitative characteristics of the obtained fractions, in particular the content of impurities (X, %) of lower-boiling components of another fraction, should come from sensors located on the pipelines of the main material flows coming from the distillation column. As controllable indicators for determining (X, %), it has been proposed to use the indicator of relative permittivity – a measure of electrical properties of both raw materials and obtained fractions, supplemented by values of physicochemical parameters such as density and kinematic viscosity. It has been experimentally established that the increasing of the content of impurities in the studied fractions of adjacent fractions with lower boiling points leads to a decrease in the values of all mentioned indicators. Based on these data, a multiple regression equations were obtained, which adequately (R2 = 0.9847 ÷ 0.9969) with an error of 0.5-1.3 % can determine the values of X in adjacent fractions. The obtained equations, in turn, allow to quickly determine the effect of the imposition of compatible fractions, which can be used in the implementation of the system of operational control of the rectification process at the hydrocarbons primary processing plants. Keywords: hydrocarbon raw materials, rectification, fractions, superposition, low-boiling impurities, operational control, dielectric constant. Corresponding author A. B. Grigorov, e-mail: grigorovandrey@ukr.net
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烃类初级加工过程的操作控制
本文探讨了解决烃类(石油、凝析油等)原料初级加工过程中出现的技术文献称之为“馏分叠加效应”的问题。这个问题与包括精馏塔在内的工艺设备的使用有关,可以通过对烃类分离成馏分过程的工艺参数(温度、压力、熔合量等)的操作控制和调节来解决。原料分馏馏分的操作控制应基于一个系统,该系统包括工艺参数(馏出馏分质量指标)的操作控制单元和可以立即将参数调整到所需水平以确保产品一定质量的校正单元。所得馏分的定性特征的主要信息,特别是另一馏分的低沸点组分的杂质(X, %)的含量,应来自位于来自精馏塔的主要物料流管道上的传感器。作为确定(X, %)的可控指标,建议使用相对介电常数指标——原料和所得组分的电学性质的度量,并辅以诸如密度和运动粘度等理化参数值。实验证明,沸点较低的相邻馏分所研究馏分中杂质含量的增加会导致上述各项指标的降低。根据这些数据,得到了一个多元回归方程,该方程(R2 = 0.9847 ÷ 0.9969)在0.5- 1.3%的误差范围内可以充分确定相邻分数中X的值。得到的方程反过来又允许快速确定相容馏分的施加效果,这可以用于在碳氢化合物初级加工厂的精馏过程的操作控制系统的实施。关键词:烃原料,精馏,馏分,叠加,低沸杂质,操作控制,介电常数。通讯作者A. B. Grigorov, e-mail: grigorovandrey@ukr.net
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