Investigation on the Interrelationship between the Chemical Composition, Heat Treatment Parameters and the Phase Transformation Process, Microstructure Evolution and the Mechanical Properties of Austempered Steel

O. Okwonna, O. Chima
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Abstract

The interrelationship between chemical composition, heat treatment parameters, and phase transformation, microstructural evolution and the mechanical properties of austempered steel was studied. Two samples of steel with different percentage composition of carbon of 0.56 and 0.76 were used for the study. They were austentized at the respective temperatures of 8000C, 8400C, 9000C and 9600C for 30 minutes. They were thereafter quenched using bitumen-palm kernel oil, and subjected to austempering isothermal heat treatment at 4200Cfor different time durations of 5, 15, 30, 45 and 60 minutes. The samples were tested for tensile strength, elongation, hardness and impact strength. They were also subjected to microstructural characterization to determine the phases in the microstructures and their effects on the properties of the developed materials. Results obtained revealed that the dominant phases in the microstructure were bainite, matensite and traces of retained austenite. It was found that decreasing austenitizing temperature yields finer grain structures with increase in tensile strength and elongation with decrease in hardness and relatively little effect on the impact strength. At any given austenitizing temperature, shorter austempering holding time yielded optimum properties in tensile strength and elongation while higher hardness values were associated with shorter holding time. These results proved that the process conditions have strong correlation with both the microstructures and the mechanical properties. It was concluded that the most promising microstructures with respect to excellent strength-ductility property are those obtained at the ausenitizing temperature range of 800 -8400C for the austempering time range of 5 – 30 minutes. These materials have potential for load bearing application while those austenitized within the range of 900 - 9600C using austempering time range of 5 – 15 minutes are candidate material for wear resistant application.
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奥氏体钢化学成分、热处理参数与相变过程、组织演变及力学性能关系的研究
研究了等温钢的化学成分、热处理参数与相变、显微组织演变及力学性能之间的相互关系。采用碳组成百分比分别为0.56和0.76的两种钢样品进行研究。分别在8000C、8400C、9000C和9600C的温度下奥氏体化30分钟。然后用沥青-棕榈仁油进行淬火,并在4200c下进行等温热处理,时间分别为5、15、30、45和60分钟。测试了试样的抗拉强度、伸长率、硬度和冲击强度。还对其进行了微观结构表征,以确定微观结构中的相及其对所制备材料性能的影响。结果表明,显微组织以贝氏体、马氏体和残余奥氏体为主。结果表明,降低奥氏体化温度,合金的抗拉强度提高,伸长率降低,晶粒细化,对合金的冲击强度影响较小。在任何给定的奥氏体化温度下,较短的奥氏体化保温时间可获得最佳的抗拉强度和伸长率,而较高的硬度值与较短的保温时间相关。结果表明,工艺条件对合金的显微组织和力学性能都有很强的相关性。结果表明,在奥氏体化温度为800 ~ 8400℃、等温时间为5 ~ 30 min时,获得的组织具有较好的强度-塑性性能。这些材料具有承载应用的潜力,而那些在900 - 9600C范围内使用5 - 15分钟奥氏体化的材料是耐磨应用的候选材料。
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