PEG-coated magnetite nanoparticles as adsorbents surface for remove methylene blue dye from aqueous solutions

Alaa Sulaiman, A. Farouk, Samir A. Salman, T. Al-Dhahir, Tagreed M Al-Saadi, E. E. Al-Abodi
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Abstract

Magnetite Nanoparticles (MNPs) of Fe3O4 have been prepared by a co-precipitation method of ferrous and ferric aqueous solution at sodium salt to controlling by the grain size of (MNPs). The prepared nanoparticles coated by polyethylene glycol, to obtain PEG-MNPs composite for the efficient removal the Methylene blue dye from the aqueous solutions. The prepared samples have characterized by several techniques like (FTIR) spectroscopy, (XRD), (AFM) and (SEM). The research testing the ability of coated magnetite as adsorbents surface for removing of methylene blue dye from the aqueous solution within variable experimental factors. The obtained data from this study revealed that high efficiency was observed and all adsorption processes well agree with Frindlesch model, the adsorption capacity increases with the pH increases, which enhances the process of dye removal.Magnetite Nanoparticles (MNPs) of Fe3O4 have been prepared by a co-precipitation method of ferrous and ferric aqueous solution at sodium salt to controlling by the grain size of (MNPs). The prepared nanoparticles coated by polyethylene glycol, to obtain PEG-MNPs composite for the efficient removal the Methylene blue dye from the aqueous solutions. The prepared samples have characterized by several techniques like (FTIR) spectroscopy, (XRD), (AFM) and (SEM). The research testing the ability of coated magnetite as adsorbents surface for removing of methylene blue dye from the aqueous solution within variable experimental factors. The obtained data from this study revealed that high efficiency was observed and all adsorption processes well agree with Frindlesch model, the adsorption capacity increases with the pH increases, which enhances the process of dye removal.
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聚乙二醇包覆磁铁矿纳米颗粒作为吸附剂表面去除水溶液中的亚甲基蓝染料
采用亚铁和三铁水溶液在钠盐下共沉淀法制备了Fe3O4磁性纳米颗粒(MNPs),并对其粒径进行了控制。所制备的纳米颗粒被聚乙二醇包覆,得到PEG-MNPs复合材料,用于有效去除水溶液中的亚甲基蓝染料。用FTIR、XRD、AFM、SEM等技术对制备的样品进行了表征。本研究在不同的实验条件下,测试了包覆磁铁矿作为吸附剂表面对水溶液中亚甲基蓝染料的去除能力。实验结果表明,吸附效率高,各吸附过程均符合Frindlesch模型,吸附量随pH的增大而增大,有利于脱除染料。采用亚铁和三铁水溶液在钠盐下共沉淀法制备了Fe3O4磁性纳米颗粒(MNPs),并对其粒径进行了控制。所制备的纳米颗粒被聚乙二醇包覆,得到PEG-MNPs复合材料,用于有效去除水溶液中的亚甲基蓝染料。用FTIR、XRD、AFM、SEM等技术对制备的样品进行了表征。本研究在不同的实验条件下,测试了包覆磁铁矿作为吸附剂表面对水溶液中亚甲基蓝染料的去除能力。实验结果表明,吸附效率高,各吸附过程均符合Frindlesch模型,吸附量随pH的增大而增大,有利于脱除染料。
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