Analysis of Different Assigned Value Determination Methods on Gauge Block Calibration Proficiency Testing

C. Hung
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Abstract

According to ISO/IEC 17043:2010, the definition of proficiency testing is evaluation of participant performance against pre-established criteria by means of interlaboratory comparisons. Thus pre-established criteria has significant impact on the evaluation of participant performance, in which assigned value attributed to a particular property of a proficiency test item and its standard deviation for proficiency assessment played the key role in the evaluation criteria. In order to understand the gauge block calibration capacity of the domestic laboratories in Taiwan, the Center for Measurement Standards / Industrial Technology Research Institute (CMS/ITRI) held and completed a gauge block calibration proficiency testing in 2016. In this proficiency testing, CMS used the calibration results from National Measurement Laboratory (NML) to determine the assigned value and its expanded uncertainty which were used to calculate the |En| values. In addition, according to ISO/IEC 13528:2015, the assigned value and its standard uncertainty can be determined according to the type and purpose of the proficiency testing scheme, including using the results from one laboratory, consensus values from participant results, etc. In order to explore the impact of choosing different methods to determine the assigned value and its expanded uncertainty for proficiency testing results, CMS recalculated the |En| values by using different assigned value determination method after the end of this proficiency testing. Thus, the narrative of this paper contains not only results of this gauge block calibration proficiency testing but also results of using different assigned value determination method to recalculate participant performance statistics.
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量块校准能力验证的不同赋值确定方法分析
根据 ISO/IEC 17043:2010,能力验证的定义是通过实验室间的比对,根据预先制定的标准对参与者的表现进行评价。因此,预先制定的标准对评价参加者的能力有重要影响,其中能力验证项目的特定属性赋值及其标准偏差在能力评价标准中起着关键作用。为了解国内实验室的量块校准能力,计量标准中心/工研院于2016年举办并完成了量块校准能力验证。在此次能力验证中,CMS利用国家计量实验室(NML)的校准结果确定分配值及其扩展不确定度,并以此计算|En|值。此外,根据 ISO/IEC 13528:2015,分配值及其标准不确定度可根据能力验证计划的类型和目的确定,包括使用一个实验室的结果、参与者结果的共识值等。为了探讨选择不同方法确定能力验证结果的赋值及其扩展不确定度的影响,CMS在本次能力验证结束后,采用不同的赋值确定方法重新计算了|En|值。因此,本文的叙述不仅包括本次量块校准能力验证的结果,还包括使用不同赋值确定方法重新计算参试人员性能统计数据的结果。
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