{"title":"Obtaining and studying the properties of cobalt- and nickel-containing nanocomposites by thermolysis, using saturated carboxylates as precedors","authors":"R. V. Saprykin, S. Semenov","doi":"10.37614/2307-5252.2021.2.5.043","DOIUrl":null,"url":null,"abstract":"Nickel (II) and cobalt (II) salts were synthesized with saturated monocarboxylic acids: butyric, valeric, nylon,enanthic, and caprylic. The obtained compounds were characterized by elemental analysis, IR spectroscopy,and differential scanning calorimetry. As a result of thermolysis of the synthesized carboxylates, nanocomposites were obtained, which were studied by scanning and transmission electron microscopy, elemental analysis, IR spectroscopy, energy dispersive X-ray spectroscopy, and X-ray phase analysis. The magnetic properties of the obtained nanocomposites have been studied.","PeriodicalId":438304,"journal":{"name":"Transaction Kola Science Centre","volume":"5 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2021-12-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Transaction Kola Science Centre","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.37614/2307-5252.2021.2.5.043","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
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Abstract
Nickel (II) and cobalt (II) salts were synthesized with saturated monocarboxylic acids: butyric, valeric, nylon,enanthic, and caprylic. The obtained compounds were characterized by elemental analysis, IR spectroscopy,and differential scanning calorimetry. As a result of thermolysis of the synthesized carboxylates, nanocomposites were obtained, which were studied by scanning and transmission electron microscopy, elemental analysis, IR spectroscopy, energy dispersive X-ray spectroscopy, and X-ray phase analysis. The magnetic properties of the obtained nanocomposites have been studied.
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