Study on Effect of Weld Cooling Rate on Fusion Zone Microstructure and Solidification Cracks in 316L Austenitic Stainless Steel

R. Santhosh, M. Aravind, M. Divya, A. Lakshminarayanan, S. Albert
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Abstract

A study on effect of cooling rate on mode of solidification and microstructure was carried out on austenitic stainless steel welds. A tube and plug of 316L stainless steel was joined using Gas Tungsten Arc Welding (GTAW) and laser welding processes. The welds were characterized using optical and Scanning Electron Microscope (SEM). The results indicate that cooling rate of the weld has significant effect on solidification mode, microstructure and solidification cracking. 316L weld joints prepared using GTAW process shows duplex microstructure of vermicular ferrite and austenite in the fusion zone. Whereas, the fusion zone of laser joint shows only single phase austenite microstructure. From these observations, it is clearly understood that the changes observed in the fusion zone microstructures of GTAW and laser welds are due to change in the mode of solidification as a result of change in the weld cooling rates. The predicted mode of solidification for GTA welds for 316L composition used in this study was Austenite-Ferrite (AF) and it was also confirmed through the microstructural observations. In laser joint, the weld has solidified in fully austenitic mode which deviates from the mode of solidification predicted by the conventional constitutional diagrams and hence modified weldability diagram was used. From this investigation, it was also found that the rapid solidification during laser welding is not completely partition less because segregation of sulphur was found using Scanning Electron Microscope – Energy Dispersive Spectroscope (SEM-EDS) along the dendrite boundaries of laser welds. High cooling rate during weld solidification which influences fully austenitic mode of solidification and micro segregation of impurities along the grain boundaries contribute to solidification cracking of welds in laser joints.
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焊缝冷却速率对316L奥氏体不锈钢熔合区组织及凝固裂纹影响的研究
研究了冷却速率对奥氏体不锈钢焊缝凝固方式和组织的影响。采用钨极气体保护焊(GTAW)和激光焊接工艺连接316L不锈钢管和插头。利用光学显微镜和扫描电镜对焊缝进行了表征。结果表明,焊缝冷却速度对凝固方式、组织和凝固裂纹均有显著影响。采用GTAW工艺制备的316L焊缝在熔合区呈现蠕形铁素体和奥氏体的双相组织。而激光接头的熔合区仅表现为单相奥氏体组织。从这些观察中可以清楚地了解到,GTAW和激光焊接的熔合区显微组织的变化是由于焊接冷却速率的变化导致的凝固方式的变化。本研究预测316L合金GTA焊缝的凝固模式为奥氏体-铁素体(AF),显微组织观察也证实了这一点。在激光焊接中,焊缝以完全奥氏体形式凝固,这与传统组织图预测的凝固模式不同,因此采用了改进的可焊性图。利用扫描电子显微镜-能谱仪(SEM-EDS)沿激光焊接枝晶边界发现了硫的偏析,从而发现激光焊接过程中的快速凝固并非完全没有分区。焊接凝固过程中的高冷却速率影响了焊缝的完全奥氏体凝固模式和杂质沿晶界的微偏析,导致了激光接头焊缝的凝固开裂。
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