Benzoic Acid Isolation from Frankincense

Elferida Sormin, N. Harefa, L. Purba, Sumiyati, Bernadetha Nadeak
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引用次数: 1

Abstract

The purpose of this study was to determine whether benzoic acid can be isolated from Frankincense by using safonification method followed by hydrolysis. The Frankincense sample used is Tapanuli Frankincense, also known as Frankincense Toba or more commonly called Haminjon. Furthermore, the results obtained are identified through chemical tests and physical tests, and to ensure that the results obtained are benzoic acid spectra tests are carried out using infrared spectroscopy (IR). The results obtained are 5.29% white crystals which based on the analysis results have a melting point of 121.2-1230C and infrared absorption data shows the data at v (cm-1): 3100-2700 (strong band) is a bound OH group; 1720-1690 (strong band) is a C = O group; 1650-1520 (weak band) is C = C aromatic; 1275 (medium band) is C-O carboxylic acid and 882.6-715 (medium band) is aromatic C-H out of the plane, so it is concluded that the white crystal obtained is benzoic acid as much as 5.29%.
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乳香中苯甲酸的分离
本研究的目的是确定用皂化-水解法从乳香中分离苯甲酸的可行性。使用的乳香样品是Tapanuli乳香,也被称为乳香多巴,或者更通常被称为Haminjon。此外,通过化学测试和物理测试对所得结果进行了鉴定,并使用红外光谱(IR)进行了苯甲酸光谱测试,以确保所得结果是正确的。根据分析结果得到5.29%的白色晶体,熔点为121.2 ~ 1230c,红外吸收数据表明,在v (cm-1): 3100 ~ 2700(强波段)处的数据为结合OH基团;1720-1690(强波段)为C = O群;1650-1520(弱带)为C = C芳族;1275(中波段)为C-O羧酸,882.6-715(中波段)为芳族C-H出面,由此得出得到的白色晶体中苯甲酸的含量高达5.29%。
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