The Influence of Combined Surface Treatmentsusing Plasma of Argon, Er:Yag Laser and Sandblasting on the Shear Bond Strength of Zirconia Core to the Veneering Ceramic – In Vitro Study

Preetham Hs, Kiran Kumar N
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Abstract

Background: Success of zirconia-based prosthesis is greatly affected by ceramic chipping and delamination due to poor bonding between zirconia framework and veneering ceramic. This study uses combination of surface treatment with Non-thermal Argon Plasma to evaluate its effect on Shear Bond Strength (SBS). Objective: The study aimed to evaluate the effect of different surface treatment using sandblasting, argon plasma, Er:YAG laser and its combination on SBS of zirconia to veneering ceramic. Material and Method: 150 milled and sintered zirconia blocks (10mm x 18mm) were subjected to various surface treatments and were randomly divided into five groups according to the surface treatment methods namely. Group 1: Argon plasma(220 V,100W and constant gas pressure 1 kg/cm2 and gas flow 8.5L/min) + Liner (E max ceram zirliner), Group 2: Atmospheric pressure argon plasma, Group 3: Sandblasting, Group 4: Sandblasting + Laser ablation ( Er:YAG ; 300mJ/pulse energy, frequency-10Hz ) + Argon plasma and Group 5: Sandblasting + Argon plasma. Specimens were subjected to shear bond strength test by a universal testing machine with a crosshead speed of 1 mm/min. The data were analysed with one-way ANOVA and Bonferoni test for multiple comparisons tests (α=0.05). Result: Highest shear bond strength value was obtained for Group 4 followed by Group 5, Group 3, Group 2 with least value obtained for Group 1. Conclusion: This study shows that sandblasting + Er:YAG + Argon plasma showed higher shear bond strength when compared to other groups.
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氩等离子体、Er:Yag激光和喷砂联合表面处理对氧化锆芯与贴面陶瓷剪切结合强度的影响
背景:由于氧化锆框架与贴面陶瓷粘结不良,导致陶瓷脱落和脱层严重影响假体的成功。本研究采用表面处理与非热氩等离子体相结合的方法来评价其对剪切结合强度(SBS)的影响。目的:研究喷砂、氩等离子体、Er:YAG激光及其组合等不同表面处理对氧化锆贴面陶瓷SBS的影响。材料与方法:对150块(10mm × 18mm)经研磨烧结的氧化锆块进行各种表面处理,按表面处理方式随机分为5组,分别为:第一组:氩气等离子体(220v,100W,恒气压1kg /cm2,流量8.5L/min) +衬里(E max陶瓷氧化锆衬里),第二组:常压氩气等离子体,第三组:喷砂,第四组:喷砂+激光烧蚀(Er:YAG;300mJ/脉冲能量,频率- 10hz) +氩等离子体,第五组:喷砂+氩等离子体。试件采用十字速度为1mm /min的万能试验机进行剪切粘结强度试验。资料分析采用单因素方差分析和Bonferoni多重比较检验(α=0.05)。结果:实验组4的剪切强度值最高,实验组5、实验组3、实验组2次之,实验组1的剪切强度值最小。结论:本研究表明喷砂+ Er:YAG +氩气等离子体比其他组具有更高的剪切结合强度。
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