Oxidization, Contamination, and Automation for High Temperature Verification of Thermocouples

Mike Imholte
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Abstract

During the process of verifying K type thermocouples at high temperatures, the sheath turns gray or breaks down and flakes off. This creates a risk of contaminants and damage to product in a vacuum braze furnace. The cost of recertifying the thermocouples and cleaning of the furnace block when a thermocouple sheath breaks down is high. After working through this process for many years, I came up with a new furnace setup that reduces the potential for contamination of product. This paper will explain the process, verification station set up, tools and materials used to reduce oxidization of the sheath material. We have updated from an inconel isotheral block furnace to an alumina isotheral block furnace. This eliminates the contamination to the reference PRT being it also has an alumina sheath. The why is when an alumina sheath is contaminated with inconel the OEM will not calibrate the PRT because of possible contamination to the silver fixed point cell. The automation improvement has reduced cost in labor and down time.
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热电偶高温验证的氧化、污染和自动化
在高温下验证K型热电偶的过程中,护套变灰或破裂脱落。这就产生了污染和损坏真空钎焊炉产品的风险。当热电偶护套损坏时,重新认证热电偶和清洗炉块的成本很高。在这个过程中工作了多年之后,我想出了一个新的炉设置,减少了产品污染的可能性。本文将阐述减少护套材料氧化的工艺流程、验证站的设置、工具和材料的使用。我们已经从铬镍铁合金等温块炉升级为氧化铝等温块炉。这消除了对参考PRT的污染,因为它也有一个氧化铝护套。原因是当氧化铝护套被铬镍铁合金污染时,OEM将不会校准PRT,因为可能会污染银固定点电池。自动化的改进降低了人工成本和停机时间。
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