Investigation of Microstructure and Tribological behavior of WE43/nano B4C Composites Produced by Spark Plasma Sintering

Ufuk Taşci, B. Bostan
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Abstract

In this study, composite samples of WE43 (Mg-4Y-3RE-Zr) reinforced with nano-B4C particles in different ratios (0.5 and 2 wt.%) were prepared by spark plasma sintering (SPS). The powders were mixed in a 3-dimensional ball mill at 300 rpm. The mixed powders were then hot pressed under 35 MPa pressure at 525 °C for 6 min. XRD and FESEM-EDS instruments were used to characterize the composite samples. Microhardness and wear tests were performed to designate the mechanical properties. It was found that the highest hardness occurred in the composite sample with 2% nano-B4C composites. It was also found that tribological properties improved with the increase of nano-B4C content.
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放电等离子烧结WE43/纳米B4C复合材料的微观结构和摩擦学性能研究
采用火花等离子烧结(SPS)法制备了不同比例(0.5 wt.%和2 wt.%)纳米b4c颗粒增强WE43 (Mg-4Y-3RE-Zr)的复合材料样品。粉末以300转/分的速度在三维球磨机中混合。将混合粉末在525℃下,在35 MPa压力下热压6 min,用XRD和FESEM-EDS仪器对复合样品进行表征。通过显微硬度和磨损试验来确定其力学性能。结果表明,添加2%纳米b4c复合材料的复合样品硬度最高。随着纳米b4c含量的增加,材料的摩擦学性能得到改善。
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