Synthesis and Characterization of Polyvinyl Alcohol/ Gelatin/ CuO Nanocomposite Film Via γ-Irradiation for Antimicrobial Application

Ahmed. M. Ismaiel, W. Salem, Mahmoud Sayed Abd El-sadek, Hassan Mohamed Salman, Hossam Mohamed Said
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Abstract

Chemistry Department, Faculty of Science, Jazan University, Jazan, KSA. Biological Department, Faculty of Science, South Valley University, Qena-83523, Egypt. Physics Department, Faculty of Science, South Valley University, Qena-83523, Egypt. Chemistry Department, Faculty of Science, South Valley University, Qena-83523, Egypt. Radiation Chemistry Department, National Center for Radiation Research and. Technology, P.O. Box 29 Nasr City, Cairo, Egypt Email address ah_ismaiel2006@yahoo.com *Corresponding author ABSTRACT Several polyvinyl alcohol (PVA)/ gelatin nano-copper oxide (nano-CuO) films were prepared by a solution casting method. Changes in the structural properties, with two different irradiation doses were subsequently investigated using TEM, SEM and FTIR. The FTIR spectrum and SEM shows a strong chemical interaction between PVA/ gelatin and nano-copper oxide (nano-CuO) with the formation of new peaks. Moreover, the results indicated that an intermolecular hydrogen bond and a chemical bond CuO-Cu were formed in the nano-CuO and PVA/ gelatin. Results showed that all the tested synthesized films have a significant growth inhibition of both Gram positive and negative bacteria and fungi,
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聚乙烯醇/明胶/ CuO纳米复合膜的合成及抗菌性能研究
吉赞大学理学院化学系,吉赞,沙特阿拉伯。南谷大学理学院生物学系,埃及Qena-83523南谷大学理学院物理系,埃及Qena-83523南谷大学理学院化学系,埃及Qena-83523国家辐射研究中心辐射化学系;摘要采用溶液浇铸法制备了几种聚乙烯醇(PVA)/明胶纳米氧化铜(nano-CuO)薄膜。随后用TEM、SEM和FTIR研究了两种不同辐照剂量下结构性能的变化。FTIR和SEM分析表明,PVA/明胶与纳米氧化铜(nano-CuO)发生了强烈的化学相互作用,形成了新的峰。结果表明,纳米cuo和PVA/明胶之间形成了分子间氢键和化学键CuO-Cu。结果表明,所有合成膜对革兰氏阳性和阴性细菌和真菌均有明显的生长抑制作用;
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