CRYSTAL STRUCTURE AND SURFACE MORPHOLOGY OF CD1-XFEXS SOLID SOLUTION-BASED THIN FILMS

Piretc Pub Date : 2023-08-25 DOI:10.36962/piretc27062023-96
Sona Mammadli, Matanat Mehrabova Sona Mammadli, Matanat Mehrabova, Niyazi Hasanov Niyazi Hasanov
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Abstract

Cd1-xFexS (x = 0.03) solid solutions were synthesized and thin films were obtained on their base by molecular beam condensation method. It was studied the effect of γ- irradiation on surface morphology, growth properties and crystal structure of obtained thin films. The characteristics of Cd1-xFexS (x = 0.03) solid solutions exposed to γ-rays at doses of 50, 100 and 150 kGy from 60Co source were characterized by XRD, SEM, EDX methods. XRD analysis showed that the orientation of crystal planes changes after γ-exposure. It was determined that the peak intensity of the (101) plane of Cd1-xFexS solid solutions increased with the radiation dose. Sizes of crystallites increased after γ-irradiation. Thus it is possible to manage some crystal properties with γ-irradiation. XRD investigations demonstrates, that thin films grown on glass substrates at substrate temperature Tsub=470 K were polycrystalline structure and thin films grown at substrate temperature Tsub =670K were monocrystalline structure. Keywords: Solid Solution, Semimagnetic Semiconductor, SEM, XRD, EDX, γ-radiation
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cd1 - xfxs固溶体薄膜的晶体结构和表面形貌
采用分子束缩合法合成了Cd1-xFexS (x = 0.03)固溶体,并在其基底上制备了薄膜。研究了γ辐照对薄膜表面形貌、生长性能和晶体结构的影响。采用XRD、SEM、EDX等方法对Cd1-xFexS (x = 0.03)固溶体在60Co源50、100和150 kGy γ射线下的特性进行了表征。XRD分析表明,γ辐照后晶体面取向发生了变化。结果表明,Cd1-xFexS固溶体的(101)面峰值强度随辐射剂量的增加而增加。经γ辐照后晶粒尺寸增大。因此,可以用γ辐照来控制某些晶体性质。XRD研究表明,在衬底温度Tsub=470 K下在玻璃衬底上生长的薄膜为多晶结构,在衬底温度Tsub= 670K下生长的薄膜为单晶结构。关键词:固溶体,半磁半导体,SEM, XRD, EDX, γ辐射
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