Effect of Knitting Pattern of PP Mesh on the Flexural Properties of Heat-cured PMMA Denture Base Resin

YERLİYURT, Kaan , EĞRİ, Sinan
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Abstract

Heat-cured polymethyl methacrylate is (PMMA) is the most common denture base material and some mechanical properties such as flexural strength and impact resistance etc. may lead to fail, besides its excellent properties. Polypropylene (PP) hernia mesh is a commercially available medical textile used in surgical repair of different types of hernia. It was aimed to investigate the effect of two different knitting patterns of PP meshes on the flexural properties of the PMMA denture base resin when they are used as reinforcement and compare with glass fiber mesh reinforced and no mesh used resins. Knitting patterns of the PP mesh structures were hexagonal honeycomb pattern and square pattern and these were used as single or double layer as reinforcement. 6 groups were established in the study: control group with no mesh and 5 reinforced groups with meshes (glass fiber mesh, single layer honeycomb patterned PP mesh, double layer honeycomb patterned PP mesh, single layer square patterned PP mesh, double layer square patterned PP mesh). A total of 60 samples with the dimensions of 65x10x3 mm, n=10 in each group were fabricated. The flexural strength, maximum deformation, and flexural modulus were determined by three-point bending test. Fracture surfaces were evaluated by scanning electron microscopy. The obtained data were statistically analyzed by two-way ANOVA test with Bonferroni corrections. The single layer square patterned PP mesh group exhibited the highest (76.67 ± 7.64 MPa), and the control group showed the lowest (63.49 ± 7.18 MPa) flexural strength values. The single layer glass fiber mesh group showed the highest (7.13 ± 0.55 mm) and the control group showed the lowest (4.72 ± 0.81 mm) maximum deformation values. The single layer glass fiber mesh group exhibited the highest (2131.87 ± 205.76 MPa), and the control group exhibited the lowest (1582.26 ± 98.63 MPa) flexural modulus values. Significant increase in flexural strength was observed in all polypropylene mesh-reinforced groups compared to the control group except double layer honeycomb patterned PP mesh group (p < 0.05). Using PP fiber mesh for reinforcement provide a very favorable aesthetic view and PP fiber mesh is concluded to be a promising material for reinforcement of heat-cured PMMA denture base resins.
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PP网织方式对热固化PMMA义齿基托树脂抗弯性能的影响
热固化的聚甲基丙烯酸甲酯(PMMA)是最常用的义齿基托材料,虽然其具有优异的性能,但某些力学性能如抗弯强度、抗冲击性能等可能会导致其失效。聚丙烯(PP)疝补片是一种市售的医用纺织品,用于手术修复不同类型的疝。研究两种不同编织方式的PP网对PMMA义齿基托树脂增强时抗弯性能的影响,并与玻璃纤维网增强树脂和无网树脂进行比较。聚丙烯网状结构的编织图案为六角形蜂窝图案和方形图案,可作为单层或双层补强。研究共设6组:不加网格的对照组和加网格的5个增强组(玻璃纤维网格、单层蜂窝图案PP网格、双层蜂窝图案PP网格、单层方形图案PP网格、双层方形图案PP网格)。共制作60个样品,尺寸为65x10x3 mm,每组n=10。弯曲强度、最大变形量和弯曲模量通过三点弯曲试验测定。用扫描电镜对断口表面进行评价。所得数据采用Bonferroni校正的双向方差分析进行统计学分析。单层方形PP网片组抗弯强度最高(76.67±7.64 MPa),对照组最低(63.49±7.18 MPa)。单层玻璃纤维网组最大变形值最高(7.13±0.55 mm),对照组最小(4.72±0.81 mm)。单层玻璃纤维网组弯曲模量最高(2131.87±205.76 MPa),对照组最低(1582.26±98.63 MPa)。与对照组相比,除双层蜂窝图案PP网组外,所有聚丙烯网增强组的抗弯强度均显著增加(p <0.05)。聚丙烯纤维网加固具有良好的美观性,是一种很有前途的用于热固化PMMA义齿基托树脂加固的材料。
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