Simulation and Experimental Validation of the Cure Process of an Epoxy-Based Encapsulant

IF 2 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Experimental Mechanics Pub Date : 2023-09-15 DOI:10.1007/s11340-023-01000-6
M. Politi, O. Breuer, Y. Cohen
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Abstract

Background

Reliable numerical predictive tools are instrumental in the high-end and robust design of encapsulated electronic assemblies. Process optimization and residual stress calculations require a rigorous cure simulation, which considers the transient chemical, thermal and mechanical constitutive behavior of the curing resin. Though this subject has been widely studied for epoxy-based composite materials, fewer studies have been presented on a non-reinforced bulk of low glass-transition temperature (Tg) resin.

Objective

This research aims to numerically and experimentally study the cure behavior and the development of residual stresses and strains in such epoxy based encapsulants.

Methods

The computational study is performed using a commercially available finite element cure process analysis software, and the experimental study is performed by a specially designed test specimen, employing various strain sensing techniques.

Results

The results show good compatibility between experimental and numerical predictions of the thermal behavior and cure-induced residual stresses, which validates the use of the simulative tool for process design. Process induced stress relaxation in the resin is numerically and experimentally demonstrated, which enables a mapping of the process stages at which full viscoelastic modeling is required. The substantial effect of chain mobility on cure shrinkage and residual stress development in this type of materials is numerically demonstrated.

Conclusion

The extensive numerical and experimental investigation of the cure process performed in this study provided insights to both process modeling and design.

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环氧树脂封装材料固化过程的模拟和实验验证
背景可靠的数值预测工具对于封装电子组件的高端和稳健设计至关重要。工艺优化和残余应力计算需要严格的固化模拟,其中要考虑固化树脂的瞬态化学、热和机械构成行为。尽管对环氧树脂基复合材料的这一主题进行了广泛研究,但对低玻璃化转变温度(Tg)树脂的非增强体的研究较少。研究结果表明,热行为和固化诱导残余应力的实验预测与数值预测之间具有良好的兼容性,这验证了在工艺设计中使用模拟工具的有效性。通过数值和实验证明了树脂中的工艺诱导应力松弛,从而可以绘制出需要建立完整粘弹性模型的工艺阶段图。本研究对固化过程进行了广泛的数值和实验研究,为过程建模和设计提供了启示。
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来源期刊
Experimental Mechanics
Experimental Mechanics 物理-材料科学:表征与测试
CiteScore
4.40
自引率
16.70%
发文量
111
审稿时长
3 months
期刊介绍: Experimental Mechanics is the official journal of the Society for Experimental Mechanics that publishes papers in all areas of experimentation including its theoretical and computational analysis. The journal covers research in design and implementation of novel or improved experiments to characterize materials, structures and systems. Articles extending the frontiers of experimental mechanics at large and small scales are particularly welcome. Coverage extends from research in solid and fluids mechanics to fields at the intersection of disciplines including physics, chemistry and biology. Development of new devices and technologies for metrology applications in a wide range of industrial sectors (e.g., manufacturing, high-performance materials, aerospace, information technology, medicine, energy and environmental technologies) is also covered.
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