Studying the Structure Properties of Copper Nanoparticles Prepared by Chemical Reduction Method

Q2 Pharmacology, Toxicology and Pharmaceutics Science and Technology Indonesia Pub Date : 2023-10-01 DOI:10.26554/sti.2023.8.4.640-646
Noora H. Al-Zobiadi, Ammar A. Habeeb, Awatif S. Jasim
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引用次数: 0

Abstract

The chemical reduction method (CRM) can produce high purity nanoparticles, it is a down-top chemical method based on the principle of salt reduction, this method is used in this work to synthesis copper nanoparticals (CuPNs) by use different concentrations of copper nitrate. The properties of the prepared nanoparticles were studied by fourier transform infrared (FTIR) and ultraviolet-visible (UV-Vis) spectroscopy were used to measure the absorbance spectra of the produced particles. According to the scanning electron microscope (SEM), the particles’ diameters range from (61.64 to 49.25) nm. According to X-ray diffraction, the particles exhibit a face monoclinic crystal structure (FCC). According to the transmission electron microscope findings, the particles are asymmetrically spherical in shape.
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化学还原法制备铜纳米颗粒的结构性质研究
化学还原法(CRM)是一种基于盐还原原理的自上而下的化学方法,可以制备出高纯度的纳米铜,本研究采用该方法通过使用不同浓度的硝酸铜来合成纳米铜。利用傅里叶变换红外光谱(FTIR)和紫外可见光谱(UV-Vis)对制备的纳米粒子的吸光度进行了测定。通过扫描电子显微镜(SEM)观察,颗粒直径在61.64 ~ 49.25 nm之间。x射线衍射结果表明,颗粒呈面单斜晶体结构(FCC)。通过透射电子显微镜观察,颗粒呈非对称球形。
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来源期刊
Science and Technology Indonesia
Science and Technology Indonesia Pharmacology, Toxicology and Pharmaceutics-Pharmacology, Toxicology and Pharmaceutics (miscellaneous)
CiteScore
1.80
自引率
0.00%
发文量
72
审稿时长
8 weeks
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