The neutron diffraction experiments under high pressure and high temperature on FENGHUANG diffractometer at CMRR

Leiming Fang, Xiping Chen, Lei Xie, Guangai Sun, Bo Chen, Shuming Peng
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Abstract

FENGHUANG diffractometer at CMRR, a high-intensity multi-section neutron powder diffractometer, has been constructed to in situ studies of materials under high pressure high temperature conditions. With development of anvils, high pressure high temperature cell assemblies, high pressure device and alignment system, we have been realized the angle-dispersive neutron diffraction data collect at the range of achievable pressures and temperatures of 0–30 GPa and 300–1500 K, with the sample size of millimeter scale. This paper describes the technical characteristics of diffractometer and related techniques for high pressure neutron diffraction experiments, and gives some scientific examples that have been recently performed on FENGHUANG. The experience gained experiments on FENGHUANG could help promote the development of high pressure techniques on neutron scattering facilities.

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在CMRR凤凰衍射仪上进行了高压高温下的中子衍射实验
凤凰衍射仪是一种高强度多截面中子粉末衍射仪,用于在高压高温条件下对材料进行原位研究。通过研制顶板、高压高温电池组件、高压装置和对准系统,实现了0 ~ 30 GPa、300 ~ 1500 K可达压力和温度范围内的角色散中子衍射数据采集,样品尺寸为毫米级。本文介绍了衍射仪的技术特点和高压中子衍射实验的相关技术,并给出了凤凰实验站最近进行的一些科学实验实例。凤凰实验所获得的经验有助于推动中子散射设备高压技术的发展。
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