Degree of conversion and physicomechanical properties of newly developed flowable composite derived from rice husk using urethane dimethacrylate monomer.

IF 1.7 4区 医学 Q3 ENGINEERING, BIOMEDICAL Proceedings of the Institution of Mechanical Engineers, Part H: Journal of Engineering in Medicine Pub Date : 2023-12-01 Epub Date: 2023-11-28 DOI:10.1177/09544119231208222
Nor Ain Fatihah Azlisham, Yanti Johari, Dasmawati Mohamad, Mohd Firdaus Yhaya, Zuliani Mahmood
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Abstract

This study evaluated the use of urethane dimethacrylate (UDMA) as a base monomer to prepare the newly developed flowable composite (FC) using nanohybrid silica derived from rice husk in comparison to bisphenol A-glycidyl methacrylate (Bis-GMA) on the degree of conversion and physicomechanical properties. The different loadings of base monomer to diluent monomer were used at the ratio of 40:60, 50:50, and 60:40. The bonding analysis confirmed the presence of nanohybrid silica in the newly developed FC. Independent t-test revealed a statistically significant increase in the degree of conversion, depth of cure and Vickers hardness of the UDMA-based FC, while surface roughness showed comparable results between the two base monomers. In conclusion, UDMA-based FC demonstrated superior performance with 60%-65% conversions, a significantly higher depth of cure exceeding 1 mm which complies with the Internal Standard of Organization 4049 (ISO 4049), and a substantial increase in Vickers hardness numbers compared to Bis-GMA-based FC, making UDMA a suitable alternative to Bis-GMA as a base monomer in the formulation of this newly developed FC derived from rice husk.

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新研制的以二甲基丙烯酸氨基甲酸乙酯为单体的稻壳可流动复合材料的转化率和物理力学性能。
本研究评价了以二甲基丙烯酸氨基甲酸乙酯(UDMA)为基础单体,利用稻壳衍生的纳米杂化二氧化硅制备新开发的可流动复合材料(FC),并比较了双酚a -甲基丙烯酸甘油酯(Bis-GMA)的转化率和物理力学性能。分别以40:60、50:50和60:40的比例添加基础单体和稀释单体。键合分析证实了新制备的FC中存在纳米杂化二氧化硅。独立t检验显示,udma基FC的转化程度、固化深度和维氏硬度在统计学上显著增加,而表面粗糙度在两种基础单体之间显示出相似的结果。综上所述,基于UDMA的FC具有60%-65%的转化率,固化深度超过1 mm,符合ISO 4049组织内部标准,并且与基于Bis-GMA的FC相比,维氏硬度值大幅增加,使UDMA成为Bis-GMA的合适替代品,作为新型稻壳衍生FC的基础单体。
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来源期刊
CiteScore
3.60
自引率
5.60%
发文量
122
审稿时长
6 months
期刊介绍: The Journal of Engineering in Medicine is an interdisciplinary journal encompassing all aspects of engineering in medicine. The Journal is a vital tool for maintaining an understanding of the newest techniques and research in medical engineering.
期刊最新文献
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