Effect of Binder Activation on in-Plane Capillary Flow in Multilayer Stacks of Carbon Fiber Fabrics

IF 2.3 4区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Applied Composite Materials Pub Date : 2023-12-21 DOI:10.1007/s10443-023-10198-6
Stefan Neunkirchen, Marcel Bender, Ralf Schledjewski
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Abstract

Binder/tackifier materials are commonly used in preforming processes to preserve the structural integrity of the preform during processing. In the following resin infusion or injection process, this additional material will influence the resin flow. While the influence on fabric permeability is thoroughly examined in scientific literature, only few studies investigate the capillary behavior. By thermal activation of the binder, the material melts and spreads across the layer’s surface or is imbibed by the rovings.

In this study, capillary rise experiments in planar direction with four different carbon fiber fabrics were performed. The tested stacks were activated at different temperature levels and compressed in a vacuum bag, one of them with additional external pressure in an autoclave. In case of no external pressure, the processing and testing conditions showed a larger influence than binder activation temperature, while autoclave-conditioned specimens showed a decreased capillary rise velocity for all levels of activation temperature. Digital microscopy images of the specimens show that molten binder can create a thin film between the layers, which prevents peripheral flow and thus forces the fluid to rise in the (angulated) capillary tubes inside the rovings.

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粘合剂活化对多层碳纤维织物叠层中平面内毛细流动的影响
预成型工艺中通常使用粘合剂/增粘材料,以保持预成型件在加工过程中的结构完整性。在接下来的树脂灌注或注射过程中,这种附加材料会影响树脂流动。虽然科学文献对织物渗透性的影响进行了深入研究,但只有少数研究对毛细管行为进行了调查。在本研究中,对四种不同的碳纤维织物进行了平面方向的毛细管上升实验。在不同的温度水平下,测试的叠层被激活并在真空袋中压缩,其中一个真空袋在高压灭菌器中带有额外的外部压力。在无外部压力的情况下,加工和测试条件比粘合剂活化温度的影响更大,而经过高压灭菌器处理的试样在所有活化温度下的毛细管上升速度都有所下降。试样的数码显微镜图像显示,熔融粘结剂可在层间形成一层薄膜,阻止外围流动,从而迫使流体在粗纱内部的(成角度的)毛细管中上升。
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来源期刊
Applied Composite Materials
Applied Composite Materials 工程技术-材料科学:复合
CiteScore
4.20
自引率
4.30%
发文量
81
审稿时长
1.6 months
期刊介绍: Applied Composite Materials is an international journal dedicated to the publication of original full-length papers, review articles and short communications of the highest quality that advance the development and application of engineering composite materials. Its articles identify problems that limit the performance and reliability of the composite material and composite part; and propose solutions that lead to innovation in design and the successful exploitation and commercialization of composite materials across the widest spectrum of engineering uses. The main focus is on the quantitative descriptions of material systems and processing routes. Coverage includes management of time-dependent changes in microscopic and macroscopic structure and its exploitation from the material''s conception through to its eventual obsolescence.
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