{"title":"Moisture Determination in CO2 Gas Cylinders for Application in Annulus Gas\nMonitoring Systems of Pressurized Heavy Water Reactors (PHWRs)","authors":"N. Raje, S. Kolay","doi":"10.2174/012210299x254766231115104920","DOIUrl":null,"url":null,"abstract":"\n\nCritical monitoring of moisture content in annulus gas is required due to its detrimental effect on the pressure tube, leading to surface corrosion and\nfinally the rupture of the pressure tube.\n\n\n\nThe present work describes a simple and reliable thermo-analytical method for the quantitative determination of moisture in CO2 gas cylinders,\nusing anhydrous barium chloride as the novel adsorbent material and simultaneous.\n\n\n\nThermogravimetry - Differential Thermal Analysis - Evolved Gas Analysis (Fourier Transformed InfraRed Spectroscopy) [TG-DTA-EGA(FTIR)]\nas determination techniques.\n\n\n\nDifferential Scanning Calorimetry (DSC) coupled with Microscopy has been used to see the surface morphological variations during the heat\ntreatment. The results of these studies are being discussed here.\n","PeriodicalId":479738,"journal":{"name":"Current Indian Science","volume":"55 8","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2023-12-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Current Indian Science","FirstCategoryId":"0","ListUrlMain":"https://doi.org/10.2174/012210299x254766231115104920","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
Abstract
Critical monitoring of moisture content in annulus gas is required due to its detrimental effect on the pressure tube, leading to surface corrosion and
finally the rupture of the pressure tube.
The present work describes a simple and reliable thermo-analytical method for the quantitative determination of moisture in CO2 gas cylinders,
using anhydrous barium chloride as the novel adsorbent material and simultaneous.
Thermogravimetry - Differential Thermal Analysis - Evolved Gas Analysis (Fourier Transformed InfraRed Spectroscopy) [TG-DTA-EGA(FTIR)]
as determination techniques.
Differential Scanning Calorimetry (DSC) coupled with Microscopy has been used to see the surface morphological variations during the heat
treatment. The results of these studies are being discussed here.